Crystal structure and X-ray powder diffraction data for Lumateperone tosylate

被引：0
|
作者：
Liu, Jiyong [1 ]
Shi, Dier [1 ]
Liu, Shuna [1 ]
Hu, Xiurong [1 ]
机构：
[1] Zhejiang Univ, Dept Chem, Hangzhou 310058, Peoples R China
来源：
POWDER DIFFRACTION | 2023年
关键词：
X-ray powder diffraction data; Lumateperone tosylate; solid-state form; preferred orientation;
D O I：
10.1017/S0885715623000337
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
X-ray powder diffraction data, unit-cell parameters, and space group for the Lumateperone tosylate, C24H29FN3O & sdot;C7H7O3S, are reported [a = 15.5848(10) angstrom, b = 6.0700(4) angstrom, c = 31.3201(14) angstrom, beta = 96.544(5)degrees, V = 2943.58 angstrom 3, Z = 4, and space group C2]. In each case, all measured lines were indexed and were consistent with the corresponding space group. The single-crystal data of Lumateperone tosylate is also reported, respectively [a = 15.626(3) angstrom, b = 6.0806(10) angstrom, c = 31.415(5) angstrom, beta = 96.609(7)degrees, V = 2965.1(8) angstrom 3, Z = 4, and space group C2]. The experimental powder diffraction pattern has been well matched with the simulated pattern derived from the single-crystal data with preferred orientation in the [002] direction (orientation coefficient = 0.75).
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页数：5
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