Crystal structure determination of zeolite N from synchrotron X-ray powder diffraction data

被引:12
|
作者
Christensen, AN [1 ]
Fjellvag, H [1 ]
机构
[1] UNIV OSLO,DEPT CHEM,N-0315 OSLO 3,NORWAY
来源
ACTA CHEMICA SCANDINAVICA | 1997年 / 51卷 / 10期
关键词
D O I
10.3891/acta.chem.scand.51-0969
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
The crystal structure of zeolite N (EDI type framework) has been refined using high-resolution synchrotron powder diffraction data. The structure is pseudotetragonal. The orthorhombic distortion is observable as a slight line broadening, a=990.41(2), b=988.60(2), c=1309.00(2) pm, space group 1222, No. 23, Z=1, for the composition K12Al10Si10O40Cl2 . 8H(2)O. The AlO4 and SiO4 tetrahedra form an ordered arrangement similar to that in edingtonite. The potassium and chlorine atoms form deformed ClK6 octahedra positioned in the channels running along [001].
引用
收藏
页码:969 / 973
页数:5
相关论文
共 50 条
  • [1] Crystal structure determination of capecitabine from X-ray synchrotron powder diffraction data
    Rohlicek, Jan
    Husak, Michal
    Kratochvil, Bohumil
    Gavenda, Ales
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : C211 - C211
  • [2] Crystal structure determination from X-ray powder diffraction data
    Tremayne, Maryjane
    [J]. ENGINEERING OF CRYSTALLINE MATERIALS PROPERTIES: STATE OF THE ART IN MODELING, DESIGN AND APPLICATIONS, 2008, : 477 - 493
  • [3] Crystal structure of nitarsone determined from synchrotron X-ray powder diffraction data
    van der Lee, A
    Richez, P
    Tapiero, C
    [J]. JOURNAL OF MOLECULAR STRUCTURE, 2005, 743 (1-3) : 223 - 228
  • [4] Unknown crystal structure determination from X-ray powder diffraction data
    Shi, Y
    Liang, JK
    Liu, QL
    Chen, XL
    [J]. SCIENCE IN CHINA SERIES A-MATHEMATICS PHYSICS ASTRONOMY, 1998, 41 (02): : 191 - 197
  • [5] The limits to the determination of crystal structure from powder X-ray diffraction data
    Solans, X
    [J]. EPDIC 7: EUROPEAN POWDER DIFFRACTION, PTS 1 AND 2, 2001, 378-3 : 80 - 85
  • [6] The limits to the determination of crystal structure from powder X-ray diffraction data
    Solans, X
    [J]. ANALES DE QUIMICA-INTERNATIONAL EDITION, 1998, 94 (06): : 406 - 409
  • [7] Unknown crystal structure determination from X-ray powder diffraction data
    施颖
    梁敬魁
    刘泉林
    陈小龙
    [J]. Science China Mathematics, 1998, (02) : 191 - 197
  • [8] Unknown crystal structure determination from X-ray powder diffraction data
    Ying Shi
    Jingkui Liang
    Quanlin Liu
    Xiaolong Chen
    [J]. Science in China Series A: Mathematics, 1998, 41 : 191 - 197
  • [9] Crystal Structure of a Polymorph of Carnidazole from Synchrotron X-ray Powder Diffraction
    de Armas, Hector Novoa
    Peeters, Maurice O.
    De Ridder, Dirk J. A.
    Schenk, Henk
    Blaton, Norbert
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2005, 61 : C337 - C337
  • [10] Ab initio crystal structure determination of two chain functionalized pyrroles from synchrotron X-ray powder diffraction data
    da Silva, Ivan
    Lopez-Tosco, Sara
    Tejedor, David
    Garcia-Tellado, Fernando
    Gonzalez-Platas, Javier
    [J]. POWDER DIFFRACTION, 2012, 27 (03) : 172 - 178