Crystal structure and Hirshfeld surface analysis of bis(μ-4-tert-butoxy-4-oxobut-2-en-2-olato)bis[(4-tert-butoxy-4-oxobut-2-en-2-olato)ethanolzinc(II)]

被引：0

作者：

Shtokvysh, Olherd O. ^{[1
]}

Dyakonenko, Viktoriya V. ^{[1
,2
]}

Koval, Lyudmila I. ^{[1
]}

Pekhnyo, Vasyl I. ^{[1
]}

机构：

[1] Natl Acad Sci Ukraine, VI Vernadskii Inst Gen & Inorgan Chem, Akad Palladin Ave 32-34, UA-03142 Kiev, Ukraine

[2] Natl Acad Sci Ukraine, SSI Inst Single Crystals, Nauki Ave 60, UA-61001 Kharkiv, Ukraine

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2023年 / 79卷

关键词：

crystal structure; complex; zinc; tertbutyl acetoacetate; keto ester; ethanol; binuclear structure; COMPLEXES; PRECURSORS; PROGRAM;

D O I：

10.1107/S2056989023003377

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecular and crystal structure of the title binuclear Zn2+ complex, [Zn-2(C8H13O3)4(C2H5OH)(2)], with enolated anionic tert-butylacetoacetate and ethanol was analysed. The coordination polyhedra of the Zn atoms are distorted octahedra formed by six oxygen atoms that belong to three ligand molecules and a coordinated ethanol molecule. In the crystal phase, alternating layers can be distinguished parallel to the ac plane. A Hirshfeld surface analysis showed that there are no strong intermolecular interactions in the structure. The most significant contributions to the overall crystal packing are from H center dot center dot center dot H intermolecular contacts.

引用

页码：478 / +

页数：10

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