From Lab to Pilot Scale: Commissioning of an Integrated Device for the Generation of Crystals

被引：3

作者：

Dobler, Timo ^{[1
]}

Hoeving, Stefan ^{[2
]}

Dreiser, Christian ^{[3
]}

Gleiss, Marco ^{[1
]}

Groeschen, Mathias ^{[3
]}

Henkel, Alexander ^{[4
]}

Hoerne, Manuel ^{[5
]}

Schaefer, Martin ^{[4
]}

Sonnenschein, Jana ^{[6
]}

Wiese, Georg ^{[7
]}

Wohlgemuth, Kerstin ^{[6
]}

Kockmann, Norbert ^{[2
]}

Nirschl, Hermann ^{[1
]}

机构：

[1] Karlsruhe Inst Technol, Inst Mech Proc Engn & Mech, Str Forum 8, D-76131 Karlsruhe, Germany

[2] TU Dortmund Univ, Lab Equipment Design, Emil Figge Str 68, D-44227 Dortmund, Germany

[3] Clariant Prod Deutschland GmbH, Brunningstr 50, D-65929 Frankfurt, Germany

[4] BHS Sonthofen GmbH, Eisenschmelze 47, D-87527 Sonthofen, Germany

[5] HiTec Zang GmbH, Ebertstr 28-32, D-52134 Herzogenrath, Germany

[6] TU Dortmund Univ, Lab Plant & Proc Design, Emil Figge Str 70, D-44227 Dortmund, Germany

[7] SONOTEC GmbH, Neuendorfer Str 2, D-06112 Halle, Germany

来源：

CHEMICAL ENGINEERING & TECHNOLOGY | 2023年 / 46卷 / 07期

关键词：

Batch-to-continuous production; Crystal generation; Integrated process design; Modularization; Plant commissioning; QUASI-CONTINUOUS PRODUCTION; PROGRESS; CRYSTALLIZATION; SEPARATION; PROFILES; PLANT;

D O I：

10.1002/ceat.202200616

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

Fast time-to-market, increased efficiency, and flexibility of production processes are major motivators for the development of integrated, continuous apparatuses with short changeover times. Following this trend, the modular belt crystallizer was developed and characterized in lab scale with the model system sucrose-water. Based on the promising results, the plant concept was upscaled and commissioned in industrial environment. The results are presented within the scope of this work. Starting from small seed crystals in solution, it was possible to grow, separate, and dry product particles. Further, the conducted experiments demonstrated that it is feasible to transfer the results from laboratory to pilot scale, which in turn enables accelerated process design as well as development.

引用

页码：1511 / 1520

页数：10

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