CRYSTAL AND MOLECULAR STRUCTURE OF 1-ETHOXYCAR-BONYLMETHYL-2 N-(DIMETHYLAMINO)THIOCARBONYL 3-PR-OPYL 2,4-DIOXO 1,3,2-BENZODIAZAPHOSPHORIN (1)

被引：0

作者：

Chen Ru-Yu Bao RongInstitute of Elemento-orgmic Chemistry

机构：

来源：

结构化学 | 1990年 / 02期

基金：

中国国家自然科学基金;

关键词：

DIMETHYLAMINO)THIOCARBONYL 3-PR-OPYL 2,4-DIOXO 1,3,2-BENZODIAZAPHOSPHORIN; CRYSTAL AND MOLECULAR STRUCTURE OF 1-ETHOXYCAR-BONYLMETHYL-2 N; PR;

D O I：

10.14102/j.cnki.0254-5861.1990.02.010

中图分类号：

学科分类号：

摘要：

The title compound,C17H24N3O4PS(Mr = 405. 42) ,is a new compound of six-membered benzoheterocycle in which the five atoms N(1),C(1),C(11),C(16) andN(2) are coplanar with the and groups in trans-cross conformations. The crystal belongs to triclinic system,space group P1,with cell parameters a = 8. 580(2),b = 10.015 (4),c= 11. 896 (4) A ,α= 90. 65(3) ,β= 105. 70(3). γ= 89. 52(3)% V = 983. 9 A3,Z=2,Dx = 1. 37g/cm3. The final refinement converged with R=0. 074,Rw = 0. 090.

引用

页码：126 / 129

页数：4

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