Synthesis and Crystal Structure of N-(2-(1,3,4-oxadiazol-2-yl)phenyl)-2,3-dimethylaniline

被引：0
|
作者：
Ali Souldozi [1 ]
Seyed Hamid Reza Shojaei [2 ]
Ali Ramazani [3 ]
Katarzyna ?lepokura
Tadeusz Lis [4 ]
机构：
[1] Department of Chemistry, Urmia Branch, Islamic Azad University
[2] Department of Physics, Urmia Branch, Islamic Azad University
[3] Department of Chemistry, Zanjan Branch, Islamic Azad University
[4] Faculty of Chemistry, University of Wroc?aw, 14 Joliot-Curie St., 50-383 Wroc?aw, Poland
来源：
Chinese Journal of Structural Chemistry | 2014年 / 33卷 / 03期
关键词：
single-crystal X-ray structure; 1; 3; 4-oxadiazoles; N-(2-(1; 4-oxadiazol-2yl)phenyl)-2; 3-dimethylaniline; (N-isocyanimino)triphenylphosphorane;
D O I：
10.14102/j.cnki.0254-5861.2014.03.011
中图分类号：
O626.2 [含双或多异原子的五节杂环];
学科分类号：
070303 ; 081704 ;
摘要：
The title compound, N-(2-(1,3,4-oxadiazol-2-yl)phenyl)-2,3-dimethylaniline, was synthesized and studied by single-crystal X-ray diffraction method. The structure of the product was confirmed by IR, 1H- and 13C-NMR spectroscopy, elemental analysis and mass spectrometry. These experimental studies were supported by theoretical optimizations.
引用
收藏
页码：407 / 414
页数：8
相关论文
共 50 条
  • [21] Polymorphism of 3-(5-phenyl-1,3,4-oxadiazol-2-yl)- and 3-[5-(pyridin-4-yl)-1,3,4-oxadiazol-2-yl]-2H-chromen-2-ones
    Shishkina, Svitlana V.
    Konovalova, Irina S.
    Trostianko, Pavlo V.
    Geleverya, Anna O.
    Kovalenko, Sergiy M.
    Bunyatyan, Natalya D.
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2019, 75 : 1541 - +
  • [22] N-Phenyl-N-{4-[5-(2-phenyl-3-pyridyl)-1,3,4-oxadiazol-2-yl]phenyl}aniline
    Han, Li-Ping
    Li, Bin
    Liu, Jie
    Liu, Qing-Chun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4780 - U5705
  • [23] Synthesis of 2-{(5-phenyl-1,3,4-Oxadiazol-2-yl)sulfanyl}-N-substituted acetamides as potential antimicrobial and hemolytic agents
    Aziz-ur-Rehman
    Abbasi, Muhammad Athar
    Siddiqui, Sabahat Zahra
    Ahmad, Irshad
    Shahid, Muhammad
    Subhani, Zinayyera
    PAKISTAN JOURNAL OF PHARMACEUTICAL SCIENCES, 2016, 29 (03) : 801 - 809
  • [24] Synthesis and local anesthetic activity of some novel N-[5-(4-substituted)phenyl-1,3,4-oxadiazol-2-yl]-2-(substituted)-acetamides
    Rajak, Harish
    Kharya, Murli Dhar
    Mishra, Pradeep
    ARCHIV DER PHARMAZIE, 2008, 341 (04) : 247 - 261
  • [25] Crystal structures of 3-methoxy-4-{[5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl]methoxy}benzonitrile and N-(4-{[5-(4-chlorophenyl)-1,3,4-oxadiazol-2-yl]methoxy}phenyl)acetamide
    Lakshmithendral, K.
    Archana, K.
    Saravanan, K.
    Kabilan, S.
    Selvanayagam, S.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 1919 - +
  • [26] N-[(E)-3,4-Dimethoxybenzylidene]-2,3-dimethylaniline
    Tahir, M. Nawaz
    Tariq, Muhammad Ilyas
    Tariq, Riaz H.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : o2378
  • [27] SYNTHESIS OF 2- AND 6-CHLORO-3-(5-METHYL-1,3,4-OXADIAZOL-2-YL)PYRIDINES
    PONTICELLO, GS
    ENGELHARDT, EL
    BALDWIN, JJ
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1980, 17 (03) : 425 - 427
  • [28] Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl]benzamide : N,N-dimethylformamide (1:1)
    Sharma, P.
    Subbulakshmi, K. N.
    Narayana, B.
    Sarojini, B. K.
    Kant, R.
    CRYSTALLOGRAPHY REPORTS, 2016, 61 (02) : 230 - 233
  • [29] One-Pot Four-Component Synthesis of N2-Alkyl-N3-[2-(1,3,4-oxadiazol-2-yl)aryl]benzofuran-2,3-diamines
    Adib, Mehdi
    Sheikhi, Ehsan
    Karimzadeh, Morteza
    Bijanzadeh, Hamid Reza
    Amanlou, Massoud
    HELVETICA CHIMICA ACTA, 2012, 95 (05) : 788 - 794
  • [30] Crystal structure of 2-(thiophen-2-yl)-1-(5-thioxo-4,5-dihydro-1,3,4-oxadiazol-2-yl)ethenyl]benzamide : N,N-dimethylformamide (1 : 1)
    P. Sharma
    K. N. Subbulakshmi
    B. Narayana
    B. K. Sarojini
    R. Kant
    Crystallography Reports, 2016, 61 : 230 - 233
12345