Determination of arylamine compounds in waste water using solid-phase extraction and reversed-phase high performance liquid chromatography

被引：0

作者：

Zhao, Shu-Li ^{[1
]}

Wei, Fu-Sheng ^{[1
]}

Zou, Han-Fa ^{[2
]}

Xu, Xiao-Bai ^{[3
]}

机构：

[1] China Natl. Environ. Monitoring Ctr., Beisihuan Dong Lu, Beijing, 100029, China

[2] Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116012, China

[3] Res. Ctr. for Eco-Environ. Sciences, Chinese Academy of Sciences, Beijing, 100085, China

来源：

Journal of Liquid Chromatography and Related Technologies | 1998年 / 21卷 / 05期

关键词：

High performance liquid chromatography - Methanol - Separation - Solvent extraction - Ultraviolet detectors - Wastewater treatment;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

A simple, rapid, and sensitive method for determining 10 arylamine compounds in wastewater sample using solid-phase extraction (SPE) and high performance liquid chromatography (HPLC) with UV detection is developed. An SPE procedure is described for extracting and preconcentrating the arylamines on Sep-Pak C18 cartridges with methanol as solvent. A mobile phase gradient of acetonitrile-water was used for the separation and determination of the arylamines. The detection limits of the compounds were in the range of 0.1-1.5 μg/L. Recoveries were 84-107% for 10 arylamines at concentration levels of 20 μg/L with relative standard deviations of less than 8% (n = 4).

引用

页码：717 / 724

共 50 条

[21] Analysis of nine food additives in wine by dispersive solid-phase extraction and reversed-phase high performance liquid chromatography
Zhao, Yong-Gang
Cai, Mei-Qiang
Chen, Xiao-Hong
Pan, Sheng-Dong
Yao, Shan-Shan
Jin, Mi-Cong
FOOD RESEARCH INTERNATIONAL, 2013, 52 (01) : 350 - 358
[22] SOLID-PHASE EXTRACTION AND OPTIMIZED SEPARATION OF DOXORUBICIN, EPIRUBICIN AND THEIR METABOLITES USING REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
NICHOLLS, G
CLARK, BJ
BROWN, JE
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 1992, 10 (10-12) : 949 - 957
[23] A simple method for nicardipine hydrochloride quantification in plasma using solid-phase extraction and reversed-phase high-performance liquid chromatography
Fernandes, CM
Veiga, FJB
BIOMEDICAL CHROMATOGRAPHY, 2003, 17 (01) : 33 - 38
[24] DETERMINATION OF BENZALKONIUM CHLORIDE IN OPHTHALMIC SOLUTIONS CONTAINING TYLOXAPOL BY SOLID-PHASE EXTRACTION AND REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
FAN, TY
WALL, GM
JOURNAL OF PHARMACEUTICAL SCIENCES, 1993, 82 (11) : 1172 - 1174
[25] Determination of glycolic acid in cosmetic products by solid-phase extraction and reversed-phase ion-pair high-performance liquid chromatography
Scalia, S
Callegari, R
Villani, S
JOURNAL OF CHROMATOGRAPHY A, 1998, 795 (02) : 219 - 225
[26] REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF CYPROHEPTADINE FROM URINE BY SOLID-PHASE EXTRACTION
KOUNTOURELLIS, JE
EBETE, KO
JOURNAL OF CHROMATOGRAPHY B-BIOMEDICAL APPLICATIONS, 1995, 664 (02): : 468 - 471
[27] SOLID-PHASE EXTRACTION AND REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF SULFUR MUSTARD IN BLOOD
DANGI, RS
JEEVARATNAM, K
SUGENDRAN, K
MALHOTRA, RC
RAGHUVEERAN, CD
JOURNAL OF CHROMATOGRAPHY B-BIOMEDICAL APPLICATIONS, 1994, 661 (02): : 341 - 345
[28] Determination of trace level microcystins in water using solid-phase extraction and high performance liquid chromatography
Zhang, WH
Xu, XQ
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2001, 29 (05) : 522 - 525
[29] Determination of three phenylurea herbicides in water using solid-phase extraction and high performance liquid chromatography
Zhao, JY
Xin, JH
Guo, YN
Cui, XJ
Zhang, M
Li, JC
CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2004, 32 (07) : 939 - 942
[30] Solid-phase extraction and reversed-phase high-performance liquid chromatography of free phenolic acids in some Echinacea species
Glowniak, K
Zgorka, G
Kozyra, M
JOURNAL OF CHROMATOGRAPHY A, 1996, 730 (1-2) : 25 - 29

← 1 2 3 4 5 →