Determination of three phenylurea herbicides in water using solid-phase extraction and high performance liquid chromatography

被引：0

作者：

Zhao, JY

Xin, JH

Guo, YN

Cui, XJ

Zhang, M

Li, JC ^{[1
]}

机构：

[1] NE Normal Univ, Fac Chem, Changchun 130024, Peoples R China

[2] Changchun Inst Biol Prod, Changchun 130062, Peoples R China

来源：

CHINESE JOURNAL OF ANALYTICAL CHEMISTRY | 2004年 / 32卷 / 07期

关键词：

phenylurea herbicide; high performance liquid chromatography; solid-phase extraction;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A high-performance liquid chromatographic ( HPLC) method for the trace analysis of phenyl urea residues in water was described. The target compounds include linuron, diuron and monuron. Water sample was subjected to solid-phase extraction (SPE) using C-18 cartridge. The analytical column of HPLC was Hypersil ODS, and the condition of HPLC was optimized: mobile phase was methanol-water (60:40, V/V), flow rate was 0.7 mL/min and temperature of column was 30degreesC. The method was simple and sensitive.

引用

页码：939 / 942

页数：4

共 7 条

[1] Diuron and its metabolites in surface water and ground water by solid phase extraction and in-vial elution
Field, JA
Reed, RL
Sawyer, TE
Martinez, M
[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (10) : 3897 - 3902
[2] Investigation into the effects of temperature and stirring rate on the solid-phase extraction of diuron from water using a C18 extraction disk
Green, CE
Abraham, MH
[J]. JOURNAL OF CHROMATOGRAPHY A, 2000, 885 (1-2) : 41 - 49
[3] HAN HY, 1998, CHINESE J CHROMATOGR, V16, P367
[4] RAPID METHOD FOR DETERMINATION OF PHENYLUREA HERBICIDES IN MILK
LAGANA, A
FAGO, G
MARION, A
PARDOMARTINEZ, B
[J]. CHROMATOGRAPHIA, 1994, 38 (1-2) : 88 - 92
[5] LI FS, 2001, CHINESE J CHROMATOGR, V19, P534
[6] Liska I, 1996, J CHROMATOGR A, V733, P235
[7] Multiresidue HPLC methods for phenyl urea herbicides in water
Ruberu, SR
Draper, WM
Perera, SK
[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2000, 48 (09) : 4109 - 4115

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