Physical, Morphological, Tensile, and Thermal Stability Characteristics of Novel Tinospora Cordifolia Natural Fiber

被引:1
|
作者
Hindi, Jamaluddin [1 ]
Muralishwara, K. [1 ]
Bhat, K. Subrahmanya [2 ]
Gurumurthy, B. M. [1 ]
Ibrahim, Ayman [1 ]
Shivaprakash, Y. M. [1 ]
机构
[1] Manipal Acad Higher Educ, Manipal Inst Technol, Dept Mech & Ind Engn, Manipal 576104, Karnataka, India
[2] Manipal Acad Higher Educ, Manipal Inst Technol, Dept Chem, Manipal, India
关键词
Tinospora cordifolia fiber; crystallinity; chemical composition; functional groups; surface morphology; single fiber tensile test; thermal stability; (sic)(sic)(sic)(sic); (sic)(sic)(sic); (sic)(sic)(sic)(sic)(sic)(sic)(sic); CELLULOSIC FIBER; BANANA PEDUNCLE; REINFORCEMENT; JUTE; PROPERTY; HEMP; FLAX;
D O I
10.1080/15440478.2024.2437539
中图分类号
TB3 [工程材料学]; TS1 [纺织工业、染整工业];
学科分类号
0805 ; 080502 ; 0821 ;
摘要
This article presents an analysis on the characterization of the natural fibers from the stem of Tinospora cordifolia plant/vine. Several characterizations/measurements were carried out on the water retted fibers to ascertain their properties. These included diameter and density measurements, X-ray Diffraction (XRD) analysis, chemical composition by gravimetric method, Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy, single fiber tensile tests, and Thermogravimetric analysis (TGA). The fibers had an average diameter of 202 mu m and density of 0.6 g/cm3. The SEM images revealed a rough surface which highlights the potential for good adhesion with the polymer matrix. The Crystalline Index (C.I) and Crystallite Size (C.S) obtained from the XRD spectra were 60.19% and 2.56 nm, respectively. Amount of cellulose, hemicellulose, lignin, and extractives in the fiber were 65%, 12%, 17%, and 6%, respectively. FTIR analysis revealed the presence of major constituents of the natural fiber such as cellulose, hemicellulose, and lignin. The tensile strength, Young's modulus, and percentage elongation at break of the fiber were 484 +/- 100 MPa, 22 +/- 4 GPa, and 3.8 +/- 1%. The onset of thermal degradation (Tonset) and maximum thermal degradation (Tmax) temperatures were 259 degrees C and 368 degrees C, respectively. Mechanical and thermal properties of the fiber were satisfactory when compared with popular natural fibers. (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)/(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic),X(sic)(sic)(sic)(sic)(XRD)(sic)(sic),(sic)(sic)(sic)(sic)(sic)(sic)(sic),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(SEM),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(FTIR),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(TGA). (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)202 mu m, (sic)(sic)(sic)0.6 g/cm3. SEM(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)XRD(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(C.I)(sic)(sic)(sic)(sic)(sic)(C.S)(sic)(sic)(sic)60.19%(sic)2.56 nm. (sic)(sic)(sic)(sic)(sic)(sic),(sic)(sic)(sic)(sic),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)65%,12%,17%(sic)6%. (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic). (sic)(sic)(sic)(sic)(sic)(sic)(sic),(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)484 +/- 100 MPa,22 +/- 4 GPa(sic)3.8 +/- 1%. (sic)(sic)(sic)(sic)(sic)(sic)(sic)(Tonset)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(Tmax)(sic)(sic)(sic)259 degrees C(sic)368 degrees C. (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic), (sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic)(sic).
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