N,N-DIALKYLCARBAMATES OF SILICON AND ALUMINUM

被引：0

作者：

DELLAMICO, DB

CALDERAZZO, F

DELLINNOCENTI, M

GULDENPFENNIG, B

IANELLI, S

PELIZZI, G

机构：

[1] UNIV PISA,DIPARTIMENTO CHIM & CHIM IND,SEZIONE CHIM INORGAN,VIA RISORGIMENTO 35,I-56126 PISA,ITALY

[2] UNIV PARMA,IST CHIM GEN,I-43100 PARMA,ITALY

[3] UNIV PARMA,CTR STRUTT DIFFRATTOMETR,CNR,I-43100 PARMA,ITALY

来源：

GAZZETTA CHIMICA ITALIANA | 1990年 / 120卷 / 12期

关键词：

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of SiCl4 with R2NH and carbon dioxide in a hydrocarbon solvent at atmospheric pressure and at room temperature gave the N,N-dialkylcarbamates Si(O2CNR2)4, R = Me, Et, (i)Pr; the iso-propyl derivative was studied by X-ray diffraction methods and found to be monomeric with terminally bonded monodentate carbamato groups. Aluminium bromide and NH(i)Pr2 under carbon dioxide led to Al2(O2CN(i)Pr2)6.

引用

页码：819 / 820

页数：2

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