SYNTHESES AND SPECTROSCOPIC CHARACTERIZATION OF STEREOISOMERS OF BIS(TERT-BUTILSULFINYL)ALKYLMETHANES

被引:0
|
作者
FRANCO, C
ZARRAGA, M
ZUNZA, H
机构
来源
关键词
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The synthesis and spectroscopic characterization of the stereoisomers of bis(tert-butilsulfinyl)methane and 1,1-bis(tert-butilsulfinyl)octane is reported. The stereoisomeric mixture of bis(tert-butilsulfinyl)methane, meso and dl pair compounds and stereoisomeric mixture of 1,1-bis(tert-butilsulfinyl)octane, were separated by chromatography and characterized by NMR techniques. The corresponding oxidation products of bis(tert-butilthio)methane: monosulfoxide, monosulfoxide-monosulfone and disulfone compounds were also synthesized.
引用
收藏
页码:319 / 324
页数:6
相关论文
共 50 条
  • [21] Syntheses and characterization of bis(silyl)alkane compounds.
    Blanton, JR
    Diminnie, JB
    Wiltz, AM
    Chen, TN
    Xue, ZL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2000, 219 : U867 - U867
  • [22] Structural and spectroscopic characterization of bis(thiosaccharinato)bis(benzimidazole)cadmium(II)
    Tarulli, S. H.
    Quinzani, O. V.
    Piro, O. E.
    Castellano, E. E.
    Baran, E. J.
    JOURNAL OF MOLECULAR STRUCTURE, 2006, 797 (1-3) : 56 - 60
  • [23] Syntheses and characterization of copper(II) complexes of bis(acetylacetone)trimethylenediimine
    Cai, YP
    Su, CY
    Xu, AW
    Kang, BS
    Tong, YX
    Liu, HQ
    Jie, S
    POLYHEDRON, 2001, 20 (7-8) : 657 - 662
  • [24] SYNTHESES OF BIS (TERT-BUTYLCYCLOPENTADIENYL) YTTERBIUM (Ⅱ) AND SAMARIUM (Ⅱ) DERIVATIVES AND THEIR CATALYTIC ACTIVITY FOR STYRENE POLYMERIZATION
    江涛
    曾东水
    沈琪
    Progress in Natural Science Communication of State Key Laboratories of China, 1991, (06) : 539 - 543
  • [25] Syntheses and characterization of structural isomers of tert-butyl/amyl-hyponitrites.
    Imonigie, JA
    Bohle, DS
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 218 : U885 - U886
  • [26] SYNTHESES, STRUCTURES AND SPECTROSCOPIC PROPERTIES OF ZIRCONIUM BIS(TETRAPHENYLPORPHYRIN) PI-RADICAL COMPLEXES
    KIM, K
    KIM, HJ
    WHANG, D
    KIM, J
    KIM, DH
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1992, 203 : 804 - INOR
  • [27] SYNTHESIS, CHARACTERIZATION, AND CHARGE-DISTRIBUTION OF BIS(4-TERT-BUTYLPYRIDINE)-BIS(3,5-DI-TERT-BUTYLQUINONE)RUTHENIUM
    HAGA, M
    DODSWORTH, ES
    LEVER, ABP
    BOONE, SR
    PIERPONT, CG
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1986, 108 (23) : 7413 - 7414
  • [28] CHEMICAL BEAM EPITAXY AND CHARACTERIZATION OF GAAS FROM BIS(TERT-BUTYLARSENIDO)DIMETHYLGALLANE DIMER AND BIS(TERT-BUTYLARSENIDO)DIETHYLGALLANE DIMER
    MILLER, JE
    EKERDT, JG
    CHEMISTRY OF MATERIALS, 1994, 6 (03) : 343 - 348
  • [29] Syntheses, Spectroscopic, Structural, Fluorescent and Thermal Properties of Bis(saccharinato)copper(II) Complexes with two Bis(pyridylamine) Ligands
    Guney, Emel
    Yilmaz, Veysel T.
    Sengul, Abdurrahman
    Buyukgungor, Orhan
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2011, 637 (02): : 246 - 250
  • [30] Silver(Ⅰ) Complexes with Mixed Diphosphine Ligands:Syntheses,Characterization and Spectroscopic Properties
    王英锋
    崔洋哲
    李中峰
    韩洪亮
    刘敏
    金琼花
    结构化学, 2017, 36 (05) : 812 - 818