(Cinnamato-kappa O-2,O')(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane-kappa N-4,N',N'',N''')nickel(II) perchlorate monohydrate

被引：0
|
作者：
Gao, Qiang [1 ]
Cao, Yi-Cheng [1 ]
机构：
[1] South China Univ Technol, Sch Biosci & Bioengn, Guangzhou 510006, Guangdong, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
D O I：
10.1107/S1600536812032175
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [Ni(C9H7O2)(C16H36N4)]ClO4 center dot H2O, the macrocyclic 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane ligand (L) folds around the Ni-II atom, which is also chelated by the carboxylate group. The geometry is a distorted N4O2 octahedron. In the crystal, adjacent molecules are connected by O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds into a zigzag chain parallel to [010].
引用
收藏
页码：M1100 / +
页数：13
相关论文
共 50 条
  • [31] meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane dihydroperchlorate monohydrate
    Hu, HM
    Sun, HS
    Huang, XY
    Chen, XH
    Liu, YJ
    You, XZ
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 588 - 590
  • [32] Crystal structure of bis[(2-(3-bromophenyl)-5-methyl-1,3-dioxane-5-carboxylato-κ-O)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4 N, N′, N", N"′)]nickel(II), C40H60Br2N4NiO8
    Tan, Ying-Zhi
    Jia, Guo-Kai
    Liu, Xiao-Wen
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (05): : 1071 - 1072
  • [33] (5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene- κ4N1,N4,N8,N11)(thiocyanato-κS)nickel(II) perchlorate monohydrate
    Bi, Jian-Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M668 - U667
  • [34] Crystal structure of bis[(2-(4-chlorophenyl)5-methyl-1,3-dioxane-5-carboxylato-κ1O) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N′")]nickel(II), C40H60Cl2N4NiO8
    Liao, Yang
    Yan, Rong-Ling
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (06): : 1215 - 1216
  • [35] Bis(cinnamato-kappa O)(1,10-phenanthroline-kappa N-2,N ')copper(II)
    Benslimane, Meriem
    Redjel, Yasmine Kheira
    Merazig, Hocine
    Daran, Jean-Claude
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M277 - +
  • [36] Crystal structure of aqua-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N‴)copper(II) 5-carboxyisophthalate tetrahydrate, C25H50N4CuO11
    Quan, Qin-Guo
    Ou, Guang-Chuan
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2024, 239 (01): : 11 - 13
  • [37] (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-1,8-diacetato)nickel(II) tetrahydrate
    Wang, SF
    Xue, JY
    Shi, L
    Zhu, HL
    Ng, SW
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M1481 - M1483
  • [38] Crystal structure of catena-poly[(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N′′′)nickel(II)-(μ2-perchlorato-κ2O:O′)] 3,5-dicarboxybenzoate methanol (1/2), C27H49ClN4NiO12
    Wang, Qiong
    Ou, Guang-Chuan
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, 237 (04): : 745 - 747
  • [39] (meso-5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) bis[O,O′-bis(4-methylphenyl) thiophosphate]
    Xiang, Yang-Guang
    Xie, Bin
    Zou, Li-Ke
    Feng, Jian-Shen
    Lai, Chuan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M59 - U672
  • [40] cis-[(7R,14R)-5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N](oxalato-κ2O,O′)nickel(II) oxalic acid solvate
    Ou, Guang-Chuan
    Dai, Yong-Qiang
    Tang, Man-Sheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M723 - U363
12345