(Cinnamato-kappa O-2,O')(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane-kappa N-4,N',N'',N''')nickel(II) perchlorate monohydrate

被引：0

作者：

Gao, Qiang ^{[1
]}

Cao, Yi-Cheng ^{[1
]}

机构：

[1] South China Univ Technol, Sch Biosci & Bioengn, Guangzhou 510006, Guangdong, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812032175

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, [Ni(C9H7O2)(C16H36N4)]ClO4 center dot H2O, the macrocyclic 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane ligand (L) folds around the Ni-II atom, which is also chelated by the carboxylate group. The geometry is a distorted N4O2 octahedron. In the crystal, adjacent molecules are connected by O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds into a zigzag chain parallel to [010].

引用

页码：M1100 / +

页数：13

共 50 条

[21] Crystal structure of (4-(4-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ2O,O′)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N"′)nickel(II) perchlorate monohydrate, C29H52Cl2N4NiO9
Liu, Fang
Jia, Guo-Kai
Ou, Guang-Chuan
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (06): : 993 - 995
[22] Crystal structure of (2-(chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylato-κ2O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N′")nickel(II) perchlorate monohydrate, Ni(C16H36N4)(C12H12O4Cl)ClO4•H2O
Ou, Guang-Chuan
Jia, Guo-Kai
Zeng, Fei
Tan, Ying-zhi
Wang, Qiong
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (03): : 369 - 370
[23] Bis(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N)(μ-L-malato-κ4O1,O2:O4,O4′)dinickel(II) bis(perchlorate) monohydrate
Ou, Guang-Chuan
Zhou, Qiang
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M728 - U413
[24] Crystal Structure of [Chlorocobalt(III)(µ-C-rac-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-N-acetato-N′, N″, N,N‴, O: O′-trichlorozinc(II)] 0.25-Hydrate
Kaliyamoorthy Panneerselvam
Tian-Huey Lu
Ta-Yung Chi
Fen-Ling Liao
Chung-Sun Chung
Analytical Sciences, 2000, 16 : 1105 - 1106
[25] Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ2O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N"′)]nickel(II) perchlorate, C29H50Cl2N4NiO8
Ou Guang-Chuan
Jia, Guo-Kai
Tan, Ying-Zhi
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (05): : 1019 - 1021
[26] (μ-C-meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-N-acetato-1κ5 N,N′,N",N′′′,O:2κO′)-tetrachloro-1κCl,2κ3 Cl-cobalt(III)zinc(II)
Panneerselvam, K
Lu, TH
Chi, TY
Tung, SF
Chung, CS
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2000, 56 : E128 - E129
[27] Diaqua(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) tetracyanidonickelate(II)
Zhang, Qian
Shen, Xiao-Ping
Zhou, Hu
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1141 - U1124
[28] cis-(Carbonato-κ2O,O′)(rac-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N)-chromium(III) bromide monohydrate
Dobrzanska, L
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M1625 - M1627
[29] (μ-C-meso-5,5,7,12,12,14-Hexa-methyl-1,4,8,11-tetraazacyclotetra-decane-N-acetato-1κ5N,N′,N″,N⌄,O:-2κO′)tetrachloro-1κCl,2κ3Cl-cobalt(III)zinc(II)
Panneerselvam, Kaliyamoorthy
Lu, Tian-Huey
Chi, Ta-Yung
Tung, Shu-Fang
Chung, Chung-Sun
Acta Crystallographica Section C: Crystal Structure Communications, 2000, 56 (04)
[30] (meso-5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N)nickel(II) [N,N-o-phenylenebis(oxamato)-κ4O,N,N′,O′]-cuprate(II) dihydrate
Gao, EQ
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : M1700 - M1702

← 1 2 3 4 5 →