(Cinnamato-kappa O-2,O')(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane-kappa N-4,N',N'',N''')nickel(II) perchlorate monohydrate

被引：0
|
作者：
Gao, Qiang [1 ]
Cao, Yi-Cheng [1 ]
机构：
[1] South China Univ Technol, Sch Biosci & Bioengn, Guangzhou 510006, Guangdong, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷
关键词：
D O I：
10.1107/S1600536812032175
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, [Ni(C9H7O2)(C16H36N4)]ClO4 center dot H2O, the macrocyclic 5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane ligand (L) folds around the Ni-II atom, which is also chelated by the carboxylate group. The geometry is a distorted N4O2 octahedron. In the crystal, adjacent molecules are connected by O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds into a zigzag chain parallel to [010].
引用
收藏
页码：M1100 / +
页数：13
相关论文
共 50 条
  • [1] (Benzoato-κ2O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N′")nickel(II) perchlorate monohydrate
    Ou, Guang-Chuan
    Zhang, Min
    Yuan, Xian-You
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M1010 - U376
  • [2] (C-rac-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetra-decane-κ4N)(nicotinato-O,O′)nickel(II) perchlorate
    Basiuk, EV
    Basiuk, VA
    Hernández-Ortega, S
    Martínez-García, M
    Saniger-Blesa, JM
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2001, 57 : 553 - 555
  • [3] cis-(Acetato-k(2)O,O')(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-k(4)N,N ',N'',N''')nickel(II) perchlorate monohydrate
    Roy, Tapashi G.
    Palit, Debashis
    Nath, Babul Chandra
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M525 - +
  • [4] 2-Aminobenzoato-κ2O,O′)(rac-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N"′)nickel(II) perchlorate monohydrate
    Ou, Guang-Chuan
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1295 - U1167
  • [5] (Acetato-O)(meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-N,N',N'',N''')zinc(II) perchlorate monohydrate
    Hu, HM
    Sun, HS
    You, XZ
    Huang, XY
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 : 1946 - 1948
  • [6] (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-1,4,8,11-tetraene-N,N′,N",N′")nickel(II) diperchlorate
    Gómez-Lara, J
    Basiuk, EV
    Basiuk, VA
    Hernández-Ortega, S
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 160 - 162
  • [7] (Benzoato-κ2O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N′")nickel(II) perchlorate benzoic acid solvate
    Ou, Guang-Chuan
    Zhang, Min
    Yuan, Xian-You
    Dai, Yong-Qiang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : M1588 - U1011
  • [8] [4-Carboxyimidazole-5-carboxylato(2-)-κ2N1,O5](5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N"′)nickel(II) monohydrate
    Ou, Guang-Chuan
    Zhou, Qiang
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1556 - U530
  • [9] Crystal structure of (4-aminobenzoato-κ2O,O′)-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4 N,N′,N",N''']nickel(II) perchlorate monohydrate, C23H44ClN5NiO7
    Ou, Guang-Chuan
    Zhou, Qiang
    Wang, Qiong
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2020, 235 (05): : 1095 - 1097
  • [10] (C-meso-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-N1-acetato-N,N′,N",N′",O)copper(II) bromide monohydrate
    Panneerselvam, K
    Lu, TH
    Chi, TY
    Chung, CS
    Chen, YJ
    Kwan, KS
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 1998, 54 : 25 - 27
12345