2-Amino-4-(2-chlorophenyl)-6-(naphthalen-1-yl)pyridine-3-carbonitrile

被引:0
|
作者
Wei, Hong-Xia [1 ]
Zhu, Jing [1 ]
Li, Ming [1 ]
Wang, Jian-qiang [1 ]
Guo, Cheng [2 ]
机构
[1] Nanjing Univ Technol, Coll Sci, Nanjing 210009, Jiangsu, Peoples R China
[2] Nanjing Univ Technol, Coll Food Sci & Light Ind, Xinmofan Rd 5, Nanjing 210009, Jiangsu, Peoples R China
关键词
single-crystal X-ray study; T= 293 K; mean sigma( C-C) = 0.007 A(degrees); R factor = 0.069; wR factor = 0.185; data-to-parameter ratio = 13.8;
D O I
10.1107/S1600536812020909
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C22H14ClN3, prepared by a one- pot reaction under microwave irradiation, the dihedral angles between the central pyridine ring and the pendant naphthyl and chlorobenzene ring systems are 49.2 (2) and 58.2 (3)(degrees), respectively. In the crystal, inversion dimers linked by pairs of N-H...N hydrogen bonds generate R-2(2) (8) loops. The pyridine N atom is the acceptor.
引用
收藏
页码:O1839 / +
页数:8
相关论文
共 50 条
  • [31] 1-(2-Chlorophenyl)-6-fluoro-2-methyl-1H-indole-3-carbonitrile
    Yang, Kun
    Li, Pei-Fan
    Liu, Yan
    Fang, Zhi-Zhong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1041 - U1467
  • [32] Synthesis and crystal structure of ethyl (2-amino-4-(2-chlorophenyl)-4H-benzo-[h]-chromene-2-yl) formate
    Wang, XS
    Shi, DQ
    Tu, SJ
    Yao, CS
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2004, 23 (03) : 278 - 281
  • [33] Pyrrolidin-1-ium 2-(naphthalen-1-yl)acetate-2-(naphthalen-1-yl)acetic acid (1/1)
    Hong, Zhao
    Yin, Fu-Jun
    Xu, Xing-You
    Han, Li-Jun
    Ren, Li
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1113 - +
  • [34] Synthesis and Crystal Structure of Ethyl (2-Amino-4-(2-chlorophenyl)-4H-benzo-[h]-chromene-2-yl) Formate
    WANG Xiang-Shana
    结构化学, 2004, (03) : 278 - 281
  • [35] Synthesis, Spectroscopic Characterization and X-ray Structure Analysis of 6-(2,5-Dichlorothiophen-3-yl)-2-methoxy-4-(4-methoxyphenyl)pyridine-3-carbonitrile
    Al-Refai, Mahmoud
    Ibrahim, Mohammad M.
    Geyer, Armin
    Marsch, Michael
    Ali, Basem F.
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2016, 46 (8-9) : 331 - 340
  • [36] Synthesis, Spectroscopic Characterization and X-ray Structure Analysis of 6-(2,5-Dichlorothiophen-3-yl)-2-methoxy-4-(4-methoxyphenyl)pyridine-3-carbonitrile
    Mahmoud Al-Refai
    Mohammad M. Ibrahim
    Armin Geyer
    Michael Marsch
    Basem F. Ali
    Journal of Chemical Crystallography, 2016, 46 : 331 - 340
  • [37] 2-amino-4-(2,4-dichlorophenyl)-6-ferrocenylpyridine-3-carbonitrile
    Tang, Zi-Qiang
    Jia, Run-Hong
    Zhang, Yan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M3125 - M3126
  • [38] 2-Methyl-6-(trifluoromethyl)imidazo[1,2-a]pyridine-3-carbonitrile
    Fun, Hoong-Kun
    Rosli, Mohd Mustaqim
    Kumar, D. J. Madhu
    Prasad, D. Jagadeesh
    Nagaraja, G. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O573 - U1315
  • [39] {2,7-Diethoxy-8-[(naphthalen-2-yl)-carbonyl]naphthalen-1-yl}(naphthalen-2-yl)methanone
    Tsumuki, Takehiro
    Okamoto, Akiko
    Oike, Hideaki
    Yonezawa, Noriyuki
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O369 - +
  • [40] SYNTHESIS AND ANTIMICROBIAL ACTIVITY OF NEW 2-(4-METHYLBENZOTHIAZOLE-2′-YL AMINO)-4-(2-CHLOROPHENYL THIOUREIDO)-6-(SUBSTITUTED THIOUREIDO)-1,3,5-TRIAZINES
    Sareen, V.
    Khatri, V.
    Jain, P.
    Sharma, K.
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2010, 20 (01) : 91 - 92