A new polymorph of 1-({[1,3-dihydroxy-2-(hydroxymethyl) propan-2-yl]iminio}methyl) naphthalen-2-olate

被引：1
|
作者：
Guo, Ailing [1 ]
Zhang, Shurong [1 ]
Wang, Kun [1 ]
Zhu, Ruitao [2 ]
机构：
[1] Shanxi Univ Tradit Chinese Med, Sch Chinese Mat Med, Taiyuan 030024, Peoples R China
[2] Taiyuan Normal Univ, Dept Chem, Taiyuan 030031, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
关键词：
Schiff base; 2-hydroxy-1-naphthaldehyde; O-H center dot center dot center dot O hydrogen bonding; N-H center dot center dot center dot O hydrogen bonding; crystal structure;
D O I：
10.1107/S205698901501539X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C15H17NO4, containing two molecules in the asymmetric unit is a polymorph of the crystal structure published by Martinez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one molecule in the asymmetric unit. Both molecules in the title compound are in the trans form. In the crystal, N-HO and O-HO hydrogen bonds connect molecules, forming a two-dimensional network parallel to (001).
引用
收藏
页码：O686 / +
页数：11
相关论文
共 50 条
  • [41] Synthesis and Properties of 1-(Alkylsulfanyl)-3-(morpholin-4-yl)propan-2-yl Arylcarbamates and Arylcarbamothioates
    K. O. K. Iskenderova
    Russian Journal of Organic Chemistry, 2021, 57 : 1979 - 1982
  • [42] Synthesis and Properties of 1-(Alkylsulfanyl)-3-(morpholin-4-yl)propan-2-yl Arylcarbamates and Arylcarbamothioates
    Iskenderova, K. O.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2021, 57 (12) : 1979 - 1982
  • [43] PRODUCTION OF (R)-1-(1,3-DITHIAN-2-YL)PROPAN-2-OL BY MICROBIAL REDUCTION
    BERNARDI, R
    CARDILLO, R
    GHIRINGHELLI, D
    DEPAVA, OV
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1987, (07): : 1607 - 1608
  • [44] Crystal structures of the 1:1 salts of 2-amino-4-nitrobenzoate with each of (2-hydroxyetnyl)di-metnyiazanium, tert-butyl(2-hydroxyethyl)azanium and 1,3-dihydroxy-2-(hydroxymethyl)propan-2-aminium
    Wardell, James L.
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 1735 - +
  • [45] 1-Benzoyl-3,3-bis(propan-2-yl)thiourea
    Gunasekaran, N.
    Karvembu, R.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2113 - U2019
  • [46] (Z)-4-[(E)-(4-Butylphenyl)diazenyl]-6-{[1,3-dihydroxy-2-(hydroxymethyl) propan-2-ylamino]methylene}-2-methoxycyclohexa-2,4-dienone
    Ersanli, CC
    Albayrak, C
    Odabasoglu, M
    Büyükgüngör, O
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O4139 - O4141
  • [47] (Z)-6-{[1,3-Dihydroxy-2-(hydroxymethyl)propan-2-ylamino]methylene}-2-methoxy-4-[(E)-o-tolyldiazenyl]cyclohexa-2,4-dienone
    Ersanli, Cem Cuneyt
    Albayrak, Cigdem
    Odabasoglu, Mustafa
    Buyukgungor, Orhan
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2006, 62 : O483 - O485
  • [48] 1-[(pyrrolidin-1-yl)(p-tolyl)methyl]naphthalen-2-ol
    Wan, Chuanwei
    Zhao, Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1926 - U3788
  • [49] [(E)-1-(Naphthalen-2-yl)ethylidene]-(naphthalen-1-ylmethyl)amine
    Bruno, Sofia M.
    Fernandes, Jose A.
    Goncalves, Isabel S.
    Paz, Filipe A. Almeida
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3143 - +
  • [50] 1-(1,3-benzothiazol-2-yl)-4,5-dihydroxy-3-phenylimidazolidin-2-one
    Olyaei, Abolfazl
    Abbasi, Alireza
    Ghandi, Mehdi
    Salimi, Farshid
    Eriksson, Lars
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O5326 - O5327
12345