A new polymorph of 1-({[1,3-dihydroxy-2-(hydroxymethyl) propan-2-yl]iminio}methyl) naphthalen-2-olate

被引：1
|
作者：
Guo, Ailing [1 ]
Zhang, Shurong [1 ]
Wang, Kun [1 ]
Zhu, Ruitao [2 ]
机构：
[1] Shanxi Univ Tradit Chinese Med, Sch Chinese Mat Med, Taiyuan 030024, Peoples R China
[2] Taiyuan Normal Univ, Dept Chem, Taiyuan 030031, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2015年 / 71卷
关键词：
Schiff base; 2-hydroxy-1-naphthaldehyde; O-H center dot center dot center dot O hydrogen bonding; N-H center dot center dot center dot O hydrogen bonding; crystal structure;
D O I：
10.1107/S205698901501539X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C15H17NO4, containing two molecules in the asymmetric unit is a polymorph of the crystal structure published by Martinez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one molecule in the asymmetric unit. Both molecules in the title compound are in the trans form. In the crystal, N-HO and O-HO hydrogen bonds connect molecules, forming a two-dimensional network parallel to (001).
引用
收藏
页码：O686 / +
页数：11
相关论文
共 50 条
  • [31] (Z)-6-{[1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl-amino]methylene}-4-[(E)-(4-ethylphenyl)diazenyl]-cyclohexa-2,4-dienone
    Sahin, O
    Albayrak, Ç
    Odabasoglu, M
    Büyükgüngör, O
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2076 - O2078
  • [32] Bis(propan-2-yl) [(1S)-1-(4-fluorophenyl)-1-hydroxy-2-nitroethyl]phosphonate
    Mandal, Tanmay
    Samanta, Sampak
    Broker, Grant A.
    Zhao, Cong-Gui
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O99 - U1897
  • [33] An Efficient Strategy for the Synthesis of 1-(Trifluoromethylsulfonamido)propan-2-yl Esters and the Evaluation of Their Cytotoxic Activity
    Gomez-Garcia, Omar
    Gomez, Elizabeth
    Monzon-Gonzalez, Cesar
    Ramirez-Apan, Teresa
    Alvarez-Toledano, Cecilio
    CHEMICAL & PHARMACEUTICAL BULLETIN, 2017, 65 (03) : 248 - 252
  • [34] Synthesis, Crystal Structure, and Hirshfeld Analysis of a Novel Schiff Base Compound 5-Hydroxy-2-{[(Propan-2-yl)Iminio]Methyl}Phenolate
    Ayyappan, A.
    Arockiasamy, S.
    JOURNAL OF STRUCTURAL CHEMISTRY, 2025, 66 (02) : 215 - 229
  • [35] Crystal structure of 7-phenyl-7-(2,4,5-trimethyl-3,6dioxocyclohexa-1,4-dien-1-yl) heptanoate 1,3-dihydroxy-2-(hydroxymethyl) propan-2-aminium monohydrate: a new solid form of seratrodast
    Lou, Benyong
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 228 - +
  • [36] 1-(1,3-Benzothiazol-2-ylsulfanyl)propan-2-olate anion as a potential multifunctional ligand in aluminum complexes
    Basiak, Dariusz
    Ochal, Zbigniew
    Justyniak, Iwona
    Ziemkowska, Wanda
    POLYHEDRON, 2015, 102 : 705 - 710
  • [37] (RP)-5-Methyl-2-(propan-2-yl)cyclohexyl phenyl{phenyl[(1-phenylethyl)amino]methyl}phosphinate
    Yang, Meng
    Sun, Yong-Ming
    Hou, Qing-Gao
    Zhao, Chang-Qiu
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02328 - +
  • [38] 1,1 '-{(Hexane-1,6-diyl)bis[(azaniumylylidene)methanylylidene]} bis(naphthalen-2-olate)
    Ouari, Kamel
    Bendia, Sabrina
    Merzougui, Moufida
    Bailly, Corinne
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O51 - +
  • [39] Crystal structure of (E)-2-chloro-6-(((1,3-dihydroxy-2-(oxidomethyl)propan-2-yl)imino) methyl)phenolate-κ3N,O,O′)manganese(IV), C22H24Cl2MnN2O8
    Xu, Xindi
    Wang, Xia
    Tian, Hui
    Wang, Man
    Wu, Qiong
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2021, 236 (02): : 391 - 392
  • [40] 1-[(Pyridin-3-yl)(pyrrolidin-1-yl)methyl]-naphthalen-2-ol
    Zhou, Qin-Qin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2614 - +
12345