A new polymorph of 1-({[1,3-dihydroxy-2-(hydroxymethyl) propan-2-yl]iminio}methyl) naphthalen-2-olate

被引:1
|
作者
Guo, Ailing [1 ]
Zhang, Shurong [1 ]
Wang, Kun [1 ]
Zhu, Ruitao [2 ]
机构
[1] Shanxi Univ Tradit Chinese Med, Sch Chinese Mat Med, Taiyuan 030024, Peoples R China
[2] Taiyuan Normal Univ, Dept Chem, Taiyuan 030031, Peoples R China
关键词
Schiff base; 2-hydroxy-1-naphthaldehyde; O-H center dot center dot center dot O hydrogen bonding; N-H center dot center dot center dot O hydrogen bonding; crystal structure;
D O I
10.1107/S205698901501539X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C15H17NO4, containing two molecules in the asymmetric unit is a polymorph of the crystal structure published by Martinez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one molecule in the asymmetric unit. Both molecules in the title compound are in the trans form. In the crystal, N-HO and O-HO hydrogen bonds connect molecules, forming a two-dimensional network parallel to (001).
引用
收藏
页码:O686 / +
页数:11
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