{[2-Methyl-2-(phenoxymethyl) propane-1,3-diyl]bis(oxy)}dibenzene

被引：0

作者：

Moussa, Ziad ^{[1
]}

Al-Masri, Harbi Tomah ^{[1
]}

Shraim, Amjed ^{[2
]}

Fettouhi, Mohammed ^{[3
]}

机构：

[1] Taibah Univ, Fac Sci, Dept Chem, POB 30002, Almadinah Almunawarrah, Saudi Arabia

[2] Qatar Univ, Coll Arts & Sci, Dept Chem & Earth Sci, Doha, Qatar

[3] King Fand Univ Petr & Minerals, Dept Chem, Dhahran 31261, Saudi Arabia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

data-to-parameter ratio = 20.2; mean σ(C-C) = 0.003 A°; R factor = 0.050; single-crystal X-ray study; T = 295 K; wR factor = 0.124;

D O I：

10.1107/S1600536814007594

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C23H24O3, was obtained in a one-step (60% yield) synthesis from 1,1,1-tris(hydroxymethyl) ethane. It features a tripodal ligand capable of complexing metal centres. One of the three conformations involving the methyl group, the central C-C bond and the phenoxy substituents is antiperiplanar while the two others are synclinal [the corresponding C-C-C-O torsion angles are -174.6 (1), -53.2 (2) and -47.3 (2)degrees]. In the crystal, C-H center dot center dot center dot O interactions link the molecules into [010] chains.

引用

页码：O539 / +

页数：8

共 50 条

[31] Synthesis and antibacterial activity of new dimeric pyridinium chlorides based on 2,2-bis(hydroxymethyl)propane-1,3-diyl spacer
Vereshchagin, A. N.
Karpenko, K. A.
Egorov, M. P.
RUSSIAN CHEMICAL BULLETIN, 2020, 69 (03) : 620 - 623
[32] Synthesis and antibacterial activity of new dimeric pyridinium chlorides based on 2,2-bis(hydroxymethyl)propane-1,3-diyl spacer
A. N. Vereshchagin
K. A. Karpenko
M. P. Egorov
Russian Chemical Bulletin, 2020, 69 : 620 - 623
[33] 2,2 '-[(4-Methyl-2-phenylimidazolidine1,3-diyl) bis(methylene)] diphenol
Rivera, Augusto
Cardenas, Lorena
Rios-Motta, Jaime
Eigner, Vaclav
Dusek, Michal
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1198 - +
[34] Protecting group manipulation on D-glucosamine propane-1,3-diyl dithioacetal
Chen, Yue-Lei
Leguijt, Robin
Redlich, Hartmut
JOURNAL OF CARBOHYDRATE CHEMISTRY, 2007, 26 (5-6) : 279 - 303
[35] Incorporation and thermal ester-interchange of bis(hydroxymethyl)propane-1,3-diyl units in PET and PBT.
Collard, DM
Kriegel, RM
Liotta, CL
Schiraldi, DA
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1998, 215 : U377 - U377
[36] Solubilities of 1,1′-(Propane-1,3-diyl)-bis(pyridinium) Dihexafluorophosphate in Dimethyl Sulfoxide plus Water
Yang, Xu-Zhao
Wang, Jun
Zhang, Zhen-Zhen
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2010, 55 (01): : 586 - 588
[37] {μ-1,1′-[2-Cyano-2-(2-pyridyl)propane-1,3-diyl]-di-η5-cyclopentadienyl}bis[tricarbonylmanganese(II)]
Duke, Charles B., III
To, Tung T.
Ross, Charles R., II
Burkey, Theodore J.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : M1848 - M1849
[38] Poly[4,4′-(propane-1,3-diyl)dipyridinium bis{tetraaquabis(μ2-5-carboxybenzene-1,2,4-tricarboxylato)bis[μ2-1,3-bis(4-pyridyl)propane]dicobalt(II)} pentahydrate]
Maria Atria, Ana
Corsini, Gino
Teresa Garland, Maria
Baggio, Ricardo
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2011, 67 : M367 - M370
[39] Apua(isothiocyanato){2,2′-[propane-1,3-diyl-bis(nitrilomethylidyne)]diphenolato}cobalt(III)
Sun, YX
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M39 - M40
[40] Di-μ-chlorido-bis[2,2′-(propane-1,3-diyl)bis(2H-benzotriazole)-κ2N1,N1′]copper(I)]
Zhou, Xiao-Li
Wang, Li-Ping
Meng, Xiang-Ru
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : M1995 - U1853

← 1 2 3 4 5 →