{[2-Methyl-2-(phenoxymethyl) propane-1,3-diyl]bis(oxy)}dibenzene

被引：0

作者：

Moussa, Ziad ^{[1
]}

Al-Masri, Harbi Tomah ^{[1
]}

Shraim, Amjed ^{[2
]}

Fettouhi, Mohammed ^{[3
]}

机构：

[1] Taibah Univ, Fac Sci, Dept Chem, POB 30002, Almadinah Almunawarrah, Saudi Arabia

[2] Qatar Univ, Coll Arts & Sci, Dept Chem & Earth Sci, Doha, Qatar

[3] King Fand Univ Petr & Minerals, Dept Chem, Dhahran 31261, Saudi Arabia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

data-to-parameter ratio = 20.2; mean σ(C-C) = 0.003 A°; R factor = 0.050; single-crystal X-ray study; T = 295 K; wR factor = 0.124;

D O I：

10.1107/S1600536814007594

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C23H24O3, was obtained in a one-step (60% yield) synthesis from 1,1,1-tris(hydroxymethyl) ethane. It features a tripodal ligand capable of complexing metal centres. One of the three conformations involving the methyl group, the central C-C bond and the phenoxy substituents is antiperiplanar while the two others are synclinal [the corresponding C-C-C-O torsion angles are -174.6 (1), -53.2 (2) and -47.3 (2)degrees]. In the crystal, C-H center dot center dot center dot O interactions link the molecules into [010] chains.

引用

页码：O539 / +

页数：8

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