{[2-Methyl-2-(phenoxymethyl) propane-1,3-diyl]bis(oxy)}dibenzene

被引：0

作者：

Moussa, Ziad ^{[1
]}

Al-Masri, Harbi Tomah ^{[1
]}

Shraim, Amjed ^{[2
]}

Fettouhi, Mohammed ^{[3
]}

机构：

[1] Taibah Univ, Fac Sci, Dept Chem, POB 30002, Almadinah Almunawarrah, Saudi Arabia

[2] Qatar Univ, Coll Arts & Sci, Dept Chem & Earth Sci, Doha, Qatar

[3] King Fand Univ Petr & Minerals, Dept Chem, Dhahran 31261, Saudi Arabia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

data-to-parameter ratio = 20.2; mean σ(C-C) = 0.003 A°; R factor = 0.050; single-crystal X-ray study; T = 295 K; wR factor = 0.124;

D O I：

10.1107/S1600536814007594

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C23H24O3, was obtained in a one-step (60% yield) synthesis from 1,1,1-tris(hydroxymethyl) ethane. It features a tripodal ligand capable of complexing metal centres. One of the three conformations involving the methyl group, the central C-C bond and the phenoxy substituents is antiperiplanar while the two others are synclinal [the corresponding C-C-C-O torsion angles are -174.6 (1), -53.2 (2) and -47.3 (2)degrees]. In the crystal, C-H center dot center dot center dot O interactions link the molecules into [010] chains.

引用

页码：O539 / +

页数：8

共 50 条

[1] 2,2′-(propane-1,3-diyl)bis(benzimidazolium) dichloride dihydrate
Hu, Bo
Deng, Xiao-Tao
Wang, Cheng-Gang
Wang, Xiao-Yan
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : M3477 - M3478
[2] N,N'-(Propane-1,3-diyl)bis(2-aminobenzamide)
Sreedasyam, Jagannatha Swamy
Sunkari, Jyothi
Kundha, Shashank
Gundapaneni, Raghava Rao
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O673 - +
[3] 2,2′-(Propane-1,3-diyl)bis(2H-indazole)
Ovalle, Saul
Bernes, Sylvain
Perez Rodriguez, Nancy
Elizondo Martinez, Perla
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2144 - U1497
[4] Propane-1,3-diyl bis(4-aminobenzoate)
Shah, Muhammad Raza
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1940 - U524
[5] 2,2′-[1,1′-(Propane-1,3-diyl)bis(nitriloethylidyne)]diphenol
Selvakumar, J.
Varghese, Babu
Raghunathan, V. S.
Nagaraja, K. S.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O1924 - O1925
[6] Propane-1,3-diyl bis-(p-toluenesulfonate)
Li, Qing-Xiang
Shen, Yun-Jun
Liu, Chang-Lin
Yu, Guo-Ping
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O2464 - O2465
[7] Propane-1,3-diyl bis(pyridine-4-carboxylate)
Brito, Ivan
Vallejos, Javier
Bolte, Michael
Lopez-Rodriguez, Matias
Cardenas, Alejandro
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1015 - U1267
[8] Propane-1,3-diyl bis(pyridine-3-carboxylate)
Brito, Ivan
Vallejos, Javier
Bolte, Michael
Lopez-Rodriguez, Matias
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O792 - U1992
[9] 2,2-Bis(hydroxymethyl)propane-1,3-diyl bis(1H-pyrrole-2-carboxylate)
Wang, JY
Yin, ZM
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O230 - O232
[10] N,N′-(Propane-1,3-diyl)bis(p-toluenesulfonamide)
Khan, Islam Ullah
Sheikh, Tahir Ali
Ejaz
Harrison, William T. A.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2371 - U600

← 1 2 3 4 5 →