QUANTITATIVE NONDESTRUCTIVE DETERMINATION OF SALICYLIC-ACID ACETATE IN ASPIRIN TABLETS BY RAMAN-SPECTROSCOPY

被引：29
|
作者：
KONTOYANNIS, CG [1 ]
ORKOULA, M [1 ]
机构：
[1] UNIV PATRAS,DEPT PHARM,GR-26500 PATRAI,GREECE
来源：
TALANTA | 1994年 / 41卷 / 11期
关键词：
D O I：
10.1016/0039-9140(94)00169-3
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Laser Raman spectroscopy was used for the quantitative determination of aspirin in aspirin-maize starch tablets. A calibration curve was constructed from spectra obtained from tablets with known quantities of aspirin and starch. The calibration curve is given from the relationship: I-552/I-478 = (W-aspirin/W-starch) x 4.21, where I-552 and I-478 and the relative Raman intensities for the 552 and 478 cm(-1) Raman shift, respectively. W-aspirin and W-starch represent the weight of aspirin and starch in a pellet.
引用
收藏
页码：1981 / 1984
页数：4
相关论文
共 50 条
  • [31] DETERMINATION OF SALICYLIC-ACID IN ASPIRIN POWDER BY 2ND DERIVATIVE ULTRAVIOLET SPECTROMETRY
    KITAMURA, K
    MAJIMA, R
    ANALYTICAL CHEMISTRY, 1983, 55 (01) : 54 - 56
  • [32] QUANTITATIVE RESONANCE RAMAN-SPECTROSCOPY
    VICKERS, TJ
    MANN, CK
    CHONG, CK
    ZHU, J
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1989, 198 : 132 - ANYL
  • [33] QUANTITATIVE RESONANCE RAMAN-SPECTROSCOPY
    VICKERS, TJ
    MANN, CK
    ZHU, JX
    CHAN, KC
    APPLIED SPECTROSCOPY REVIEWS, 1991, 26 (04) : 341 - 375
  • [34] DETERMINATION OF SALICYLIC ACID IN ASPIRIN
    STRODE, CW
    STEWART, FN
    SCHOTT, HO
    COLEMAN, OJ
    ANALYTICAL CHEMISTRY, 1957, 29 (08) : 1184 - 1186
  • [35] A NEW SPECTROPHOTOMETRIC METHOD FOR THE DETERMINATION OF FREE SALICYLIC-ACID IN ASPIRIN AND ITS FORMULATIONS BASED ON OXIDATIVE COUPLING OF 3-METHYLBENZTHIAZOLINONE-2-HYDRAZONE WITH SALICYLIC-ACID
    GEETA, N
    BAGGI, TR
    MICROCHEMICAL JOURNAL, 1988, 38 (02) : 236 - 240
  • [36] INDIRECT AAS DETERMINATION OF SALICYLIC-ACID IN PHARMACEUTICALS
    CHATTARAJ, S
    DAS, AK
    INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 1993, 32 (11): : 1009 - 1011
  • [37] Quantitative nondestructive methods for the determination of ticlopidine in tablets using reflectance near-infrared and Fourier transform Raman spectroscopy
    Markopoulou, C. K.
    Koundourellis, J. E.
    Orkoula, M. G.
    Kontoyannis, C. G.
    APPLIED SPECTROSCOPY, 2008, 62 (02) : 251 - 257
  • [38] EFFECT OF ACETYL SALICYLIC-ACID (ASPIRIN) ON LUNG SURFACTANT OF RATS
    BALASUBRAMANIAN, A
    RAMAKRISHNAN, S
    KRISHNAN, B
    RAO, AS
    INDIAN JOURNAL OF EXPERIMENTAL BIOLOGY, 1979, 17 (08) : 825 - 826
  • [39] RAPID SIMULTANEOUS DETERMINATION OF SALICYLIC ACID AND ASPIRIN BY GC .1. ANALYSIS OF SYNTHETIC ASPIRIN-SALICYLIC ACID MIXTURES AND OF SINGLE-COMPONENT ASPIRIN TABLETS
    WATSON, JR
    CRESCUOLO, P
    MATSUI, F
    JOURNAL OF PHARMACEUTICAL SCIENCES, 1971, 60 (03) : 454 - +
  • [40] NEW SPECTROPHOTOMETRIC DETERMINATION METHOD OF SALICYLIC-ACID
    BALICA, G
    PIRVANESCU, H
    PETRESCU, V
    REVISTA DE CHIMIE, 1978, 29 (08): : 780 - 780
12345