LIQUID-CHROMATOGRAPHIC ASSAY OF XYLAZINE IN SHEEP AND CATTLE PLASMA

被引：3
|
作者：
PSOMAS, JE
FLETOURIS, DJ
机构：
[1] Laboratories of Food Hygiene, School of Veterinary Medicine and Milk and Milk Products, Aristotle University, 54006, Thessaloniki
来源：
JOURNAL OF LIQUID CHROMATOGRAPHY | 1992年 / 15卷 / 09期
关键词：
D O I：
10.1080/10826079208018307
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A high-performance liquid chromatographic method for the determination of xylazine in sheep and cattle plasma at levels as low as 3 ng/ml has been developed. Xylazine was extracted from plasma under alkaline conditions with diethyl ether and, then, reextracted into phosphoric acid. Following addition of octane-1-sulfonate xylazine was extracted as ion pair into chloroform and analyzed on a reversed-phase C18, 5-mu-m, column. Overall mean recovery of the method was found to be 99 +/- 2.6%.
引用
收藏
页码：1543 / 1551
页数：9
相关论文
共 50 条
  • [21] HIGH-PRESSURE LIQUID-CHROMATOGRAPHIC ASSAY OF NETILMICIN IN PLASMA
    PENG, GW
    JACKSON, GG
    CHIOU, WL
    ANTIMICROBIAL AGENTS AND CHEMOTHERAPY, 1977, 12 (06) : 707 - 709
  • [22] LIQUID-CHROMATOGRAPHIC ASSAY OF ISOXICAM IN HUMAN-PLASMA AND URINE
    BURY, RW
    JOURNAL OF CHROMATOGRAPHY, 1985, 337 (01): : 156 - 159
  • [23] HIGH-PRESSURE LIQUID-CHROMATOGRAPHIC ASSAY FOR GRISEOFULVIN IN PLASMA
    MEYER, MC
    RAGHOW, G
    JOURNAL OF PHARMACEUTICAL SCIENCES, 1979, 68 (09) : 1127 - 1130
  • [24] LIQUID-CHROMATOGRAPHIC DETERMINATION OF DESFUROYLCEFTIOFUR METABOLITE OF CEFTIOFUR AS RESIDUE IN CATTLE PLASMA
    JAGLAN, PS
    COX, BL
    ARNOLD, TS
    KUBICEK, MF
    STUART, DJ
    GILBERTSON, TJ
    JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 1990, 73 (01): : 26 - 30
  • [25] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ASSAY FOR THE MEASUREMENT OF ATOVAQUONE IN PLASMA
    DEANGELIS, DV
    LONG, JD
    KANICS, LL
    WOOLLEY, JL
    JOURNAL OF CHROMATOGRAPHY B-BIOMEDICAL APPLICATIONS, 1994, 652 (02): : 211 - 219
  • [26] RAPID AND SENSITIVE LIQUID-CHROMATOGRAPHIC ASSAY OF MEFENAMIC-ACID IN PLASMA
    POIRIER, JM
    LEBOT, M
    CHEYMOL, G
    THERAPEUTIC DRUG MONITORING, 1992, 14 (04) : 322 - 326
  • [27] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ASSAY FOR BUMETANIDE IN PLASMA AND URINE
    SMITH, DE
    JOURNAL OF PHARMACEUTICAL SCIENCES, 1982, 71 (05) : 520 - 523
  • [28] NEW HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ASSAY FOR PLASMA DOXORUBICIN
    KOTAKE, AN
    VOGELZANG, NJ
    LARSON, RA
    CHOPORIS, N
    JOURNAL OF CHROMATOGRAPHY, 1985, 337 (01): : 194 - 200
  • [29] IMPROVED HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC ASSAY OF IBUPROFEN IN PLASMA
    SHAH, A
    JUNG, D
    JOURNAL OF CHROMATOGRAPHY, 1985, 344 (NOV): : 408 - 411
  • [30] LIQUID-CHROMATOGRAPHIC ASSAY OF BRASSINOSTEROIDS IN PLANTS
    GAMOH, K
    TAKATSUTO, S
    JOURNAL OF CHROMATOGRAPHY A, 1994, 658 (01) : 17 - 25
12345