(2R,3R)-1,4-Dioxaspiro[4.4]nonane-2,3-dicarboxylic and (2R, 3R)-1,4-dioxaspiro[4.5]decane-2,3-dicarboxylic acids

被引：0

作者：

Minyaev, Mikhail E. ^{[1
]}

Roitershtein, Dmitrii M. ^{[1
,2
]}

Vinogradov, Alexey A. ^{[1
]}

Ananyev, Ivan V. ^{[3
]}

Nifant'ev, Ilya E. ^{[1
,4
]}

机构：

[1] Russian Acad Sci, AV Topchiev Inst Petrochem Synth, 29 Leninsky Prospect, Moscow 119991, Russia

[2] Russian Acad Sci, ND Zelinsky Inst Organ Chem, 47 Leninsky Prospect, Moscow 119991, Russia

[3] Russian Acad Sci, AN Nesmeyanov Inst Organoelement Cpds, 28 Vavilova Str, Moscow 119991, Russia

[4] Moscow MV Lomonosov State Univ, Dept Chem, 1 Leninskie Gory Str,Bldg 3, Moscow 119991, Russia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2018年 / 74卷

关键词：

tartric acid; 1,3-dioxolane; ketals; NMR; hydrogen bonding; crystal structure;

D O I：

10.1107/S2056989018009593

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compounds, C9H12O6 and C10H14O6, were formed by careful hydrolysis of the corresponding diethyl esters. Their single crystals were grown from an ethyl acetate/hexane mixture. Crystals of both compounds have monoclinic (P2(1)) symmetry with a single molecule in the asymmetric unit. Both crystal structures are very similar and display four -CO-OH center dot center dot center dot O=C(OH)-hydrogen bonds, forming a two-dimensional double-layered framework.

引用

页码：1058 / +

页数：13

共 50 条

[41] Microbial Routes to (2R, 3R)-2,3-Butanediol: Recent Advances and Future Prospects
Xie, Neng-Zhong
Chen, Xian-Rui
Wang, Qing-Yan
Chen, Dong
Du, Qi-Shi
Zhou, Guo-Ping
Huang, Ri-Bo
CURRENT TOPICS IN MEDICINAL CHEMISTRY, 2017, 17 (21) : 2433 - 2439
[42] Synthesis of 2-substituted (±)-(2R, 3R, 5R)-tetrahydrofuran-3,5-dicarboxylic acid derivatives
Wang, GT
Wang, SD
Chen, YW
Gentles, R
Sowin, T
JOURNAL OF ORGANIC CHEMISTRY, 2001, 66 (06): : 2052 - 2056
[43] Engineered Serratia marcescens for efficient (3R)-acetoin and (2R,3R)-2,3-butanediol production (vol 42, pg 779, 2015)
Bai, Fangmin
Dai, Lu
Fan, Jiying
Truong, Ngoctu
Rao, Ben
Zhang, Liaoyuan
Shen, Yaling
JOURNAL OF INDUSTRIAL MICROBIOLOGY & BIOTECHNOLOGY, 2015, 42 (06) : 977 - 977
[44] 1,10-phenanthroline (2R,3R)-tartaric acid trihydrate
Wang, ZL
Li, MX
Wei, LH
Wang, JP
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2508 - O2509
[45] 1:1 and 2:1 inclusion complexes of (R,R)-(-)-trans-2,3-bis(hydroxydiphenyl-methyl)-1,4-dioxaspiro[4.4]nonane with N-allylfuran-2-carboxanilide which upon irradiation in the solid state give (-)- and (+)-photocyclization products, respectively
Department of Applied Chemistry, Faculty of Engineering, Ehime University, Matsuyama, Ehime 790, Japan
J. Org. Chem., 19 (6490-6491):
[46] Hydrogen bonding in (2R,3R)-(+)-2,3-dimethoxybutanedioic acid [(+)-tartaric acid dimethyl ether]
Gerkin, RE
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 209 - 211
[47] 2,3-di-p-toluoyl-(2R,3R)-tartaric acid ethyl acetate solvate
Tang, LD
Duan, GY
Zhang, DT
Wang, JW
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O1685 - O1686
[48] Diastereoselective synthesis of (1S,2S,3R,4R) and (1R,2S,3R,4S)-bicyclo[2.2.1]hept-2-amino-2,3-dicarboxylic acids: New conformationally-constrained (S)-aspartic acid analogues
Bunuel, E
Cativiela, C
DiazdeVillegas, MD
TETRAHEDRON-ASYMMETRY, 1996, 7 (05) : 1521 - 1528
[49] Host compounds (+)-(2R,3R)-1,1,4,4-tetraphenylbutane-1,2,3,4-tetraol (TETROL) and (2R,3R)-(-)-2,3-dimethoxy-1,1,4,4-tetraphenylbutane-1,4-diol (DMT) with guests o-, m- and p- toluidine: A comparative investigation
Barton, Benita
Dorfling, Sasha-Lee
Hosten, Eric C.
Pohl, Pieter L.
TETRAHEDRON, 2018, 74 (22) : 2754 - 2761
[50] SYNTHESIS OF (3R)-3-HYDROXY-2-HEXANONE, (2R,3R)-2,3-HEXANEDIOL AND (2S,3R)-2,3-HEXANEDIOL, THE MALE SEX-PHEROMONE OF HYLOTRUPES-BAJULUS AND PYRRHIDIUM-SANGUINEUM (CERAMBYCIDAE)
SCHRODER, F
FETTKOTHER, R
NOLDT, U
DETTNER, K
KONIG, WA
FRANCKE, W
LIEBIGS ANNALEN DER CHEMIE, 1994, (12): : 1211 - 1218

← 1 2 3 4 5 →