4-Hydroxy-3-methoxybenzaldehyde thiosemicarbazone

被引:6
|
作者
de Oliveira, Adriano Bof [1 ]
Santos Feitos, Barbara Regina [1 ]
Nather, Christian [2 ]
Jess, Inke [2 ]
机构
[1] Univ Fed Sergipe, Dept Quim, Av Marechal Rondon S-N Campus, BR-49100000 Sao Cristovao, SE, Brazil
[2] Christian Albrechts Univ Kiel, Inst Anorgan Chem, D-24118 Kiel, Germany
关键词
D O I
10.1107/S1600536813032303
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C9H11N3S, there is an intramolecular O-H center dot center dot center dot O hydrogen bond involving the OH group and the adjacent methoxy O atom. The molecule is essentially planar, with the maximum deviation from the mean plane of the nonH atoms being 0.1127 (14) angstrom for the methyl C atom. In the crystal, molecules are connected via centrosymmetric pairs of N-H center dot center dot center dot S and O-H center dot center dot center dot O hydrogen bonds into a twodimensional network parallel to (10 (3) over bar).
引用
收藏
页码:O1861 / +
页数:7
相关论文
共 50 条
  • [31] Synthesis, geometrical, spectral and anti bacterial studies of 4-hydroxy-3--methoxybenzaldehyde thiosemicarbazone by experimental and theoretical investigations
    Swaminathan, J.
    Anbusrinivasan, P.
    Vijayalakshmi, A.
    COMPUTATIONAL AND THEORETICAL CHEMISTRY, 2023, 1229
  • [32] REGIOSELECTIVE BROMINATION OF 3-HYDROXY-4-METHOXYBENZALDEHYDE
    BULAVKA, VN
    TOLKACHEV, ON
    SHAVLINSKY, AN
    KHIMIKO-FARMATSEVTICHESKII ZHURNAL, 1991, 25 (02): : 46 - 48
  • [33] 4-Hydroxy-3-iodo-5-methoxybenzaldehyde
    Zhou, Qing-Li
    Wang, Chang-Lu
    Jing, Zuo-Liang
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2795 - U1833
  • [34] 3-Hydroxy-4-methoxybenzaldehyde isonicotinoylhydrazone monohydrate
    Liu, HM
    Zhang, WQ
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3775 - O3777
  • [35] Vibrational spectra, thermodynamic parameters and fungicidal activity of 2-hydroxy-3-methoxybenzaldehyde thiosemicarbazone
    Yadav, BS
    Kumar, V
    Yadav, MK
    INDIAN JOURNAL OF PURE & APPLIED PHYSICS, 1998, 36 (10) : 557 - 566
  • [36] 2-Chloro-3-hydroxy-4-methoxybenzaldehyde
    Xuan, RC
    Zhou, Y
    Wan, YH
    Xuan, RR
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1710 - O1711
  • [37] INHIBITION OF BIOFILM FORMATION AND QUORUM SENSING- CONTROLLED VIRULENCE FACTORS OF CARIOGENIC ORAL PATHOGEN STREPTOCOCCUS MUTANS BY 4-HYDROXY-3-METHOXYBENZALDEHYDE
    Ganesh, P. Sankar
    Girija, A. Smiline
    Sankar, S.
    Shoba, G.
    Shankar, E. M.
    INTERNATIONAL JOURNAL OF INFECTIOUS DISEASES, 2023, 130 : S112 - S112
  • [38] Crystal structure of (E,E)-4-hydroxy-3-methoxybenzaldehyde azine - a second polymorph, C16H16N2O4
    Schmitt, Bonell
    Gerber, Thomas I. A.
    Hosten, Eric C.
    Betz, Richard
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2014, 229 (04): : 470 - 472
  • [39] SYNTHESIS AND CHARACTERIZATION OF COMPLEXES OF (4-METHOXYBENZALDEHYDE)-4-PHENYL-3-THIOSEMICARBAZONE
    KINTHADA, PMMS
    INORGANICA CHIMICA ACTA, 1988, 141 (02) : 179 - 183
  • [40] Investigation of aggregation induced emission in 4-hydroxy-3-methoxybenzaldehyde azine and polyazine towards application in (opto) electronics: synthesis, characterization, photophysical and electrical properties
    Dineshkumar, Sengottuvelu
    Muthusamy, Athianna
    DESIGNED MONOMERS AND POLYMERS, 2017, 20 : 234 - 249