Analytical method of polycyclic aromatic hydrocarbons (PAHs) in oil contaminated soils

被引:0
|
作者
Yoon, Jeong Ki [1 ]
Park, Jin Soo [2 ]
Shin, Sun Kyoung [2 ]
Kim, Tae Seung [1 ]
机构
[1] Natl Inst Environm Res, Soil & Groundwater Div, Incheon 404708, South Korea
[2] Natl Inst Environm Res, Organ Anal Div, Incheon 404708, South Korea
来源
ANALYTICAL SCIENCE AND TECHNOLOGY | 2008年 / 21卷 / 04期
关键词
PAHs; GC/MSD; oil contaminated soil;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This study was performed to establish an analytical method of PAHs in oil contaminated soil of these methods by evaluating the PAHs test methods from US EPA and ISO etc. The application to domestic contaminated soil leads to a conclusion that alumina column is a more effective clean-up procedure for oil contaminated soil rather than the others. It is proposed with the new analytical method of 12 PAHs except for more volatile compounds (naphthalene, acenaphthylene, acenaphthene, fluorene). The recovery of PAHs in this method ranged 67 similar to 107%. The oil contaminated soil samples were analyzed using GC/MSD. The concentration of PAHs ranged 78.68 similar to 275.57 mu g/kg. The predominated compounds were fluoranthene, pyrene and chrysene attributing about 70% of total concentration. The level of Benzo[a] pyrene ranged 1.76 similar to 24.65 mu g/kg.
引用
收藏
页码:296 / 303
页数:8
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