4,4 '-({[(Pyridine-2,6-diyl)bis(methylene)]bis(oxy)}bis(methylene))dibenzonitrile

被引：0
|
作者：
Yamin, Bohari M. [1 ]
Kamalulazmy, Nurul A. [1 ]
Hassan, Nurul I. [1 ]
机构：
[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷
关键词：
data-to-parameter ratio = 14.3; mean σ(C-C) = 0.002 Å; R factor = 0.039; single-crystal X-ray study; T = 296 K; wR factor = 0.106;
D O I：
10.1107/S1600536814000245
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The complete title molecule, C23H19N3O2, is generated by a twofold axis passing through the central ring. The two oxymethylbenzonitrile arms are attached at the meta positions of the central pyridine ring. The dihedral angle between the pyridine ring and benzene ring of both arms is 84.55 (6)degrees while the benzene rings make a dihedral angle of 46.07 (7)degrees. In the crystal, weak C-H center dot center dot center dot pi interactions link the molecules sheets parallel to the ac plane.
引用
收藏
页码：0132 / +
页数：6
相关论文
共 50 条
  • [31] DETERMINATION OF THE N-ACETYL METABOLITES OF 4,4'-METHYLENE DIANILINE AND 4,4'-METHYLENE-BIS(2-CHLOROANILINE) IN URINE
    COCKER, J
    BOOBIS, AR
    DAVIES, DS
    BIOMEDICAL AND ENVIRONMENTAL MASS SPECTROMETRY, 1988, 17 (03): : 161 - 167
  • [32] Bis(μ-ethyl pyridine-2,6-dicarboxylato)bis[diaquachlorocadmium(II)] dihydrate
    Yang, E
    Li, ZJ
    Zhang, J
    Chen, YB
    Yao, YG
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 (09): : M457 - M459
  • [33] 3,3′-(Pyridine-2,6-diyl)bis(4-allyl-4,5-dihydro-1H-1,2,4-triazole-5-thione)
    Cetin, Ahmet
    Dincer, Muharrem
    Ozdemir, Namik
    Dayan, Osman
    Cansiz, Ahmet
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4385 - O4387
  • [34] Piperazinediium bis[bis(pyridine-2,6-dicarboxylato)ferrate(III)] monohydrate
    Aghabozorg, Hossein
    Nemati, Andya
    Derikvand, Zohreh
    Ghadermazi, Mohammad
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M2921 - U581
  • [35] FATE OF MBOCA [4,4'-METHYLENE-BIS (2-CHLOROANILINE)] IN SOIL
    VOORMAN, R
    PENNER, D
    ARCHIVES OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1986, 15 (05) : 595 - 602
  • [36] SULFAMIC ACID CLEANING SOLUTION FOR 4,4'-METHYLENE-BIS-ORTHOCHLOROANILINE (MOCA)
    SCHMITT, CR
    CAGLE, GW
    AMERICAN INDUSTRIAL HYGIENE ASSOCIATION JOURNAL, 1975, 36 (03): : 181 - 186
  • [37] Cancer incidence and exposure to 4,4'-methylene-bis-ortho-chloroaniline (MbOCA)
    Dost, Abid
    Straughan, J. K.
    Sorahan, Tom
    OCCUPATIONAL MEDICINE-OXFORD, 2009, 59 (06): : 402 - 405
  • [38] Synthesis and Antibacterial Activity of Novel 5,5′-(Pyridine-2,6-Diyl)bis(4-Arylideneamino-3-Mercapto-1,2,4-Triazole) Derivatives
    Xiao, Haihua
    Li, Pingliang
    Hu, Jinhui
    Li, Ruixia
    Wu, Limin
    Guo, Dongcai
    APPLIED BIOCHEMISTRY AND BIOTECHNOLOGY, 2014, 172 (04) : 2188 - 2196
  • [39] METABOLISM OF "4,4'-METHYLENE-BIS(2-CHLOROANILINE) (MOCA) IN RATS
    MORTON, KC
    PROCEEDINGS OF THE AMERICAN ASSOCIATION FOR CANCER RESEARCH, 1983, 24 (MAR): : 83 - 83
  • [40] PLANT UPTAKE OF MBOCA [4,4'-METHYLENE-BIS (2-CHLOROANILINE)]
    VOORMAN, R
    PENNER, D
    ARCHIVES OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 1986, 15 (05) : 589 - 593
12345