N-[Ethyl(2-hydroxyethyl) carbamothioyl]3-fluorobenzamide

被引：1

作者：

Awang, Nor Wahida. ^{[1
]}

Hasbullah, Siti Aishah ^{[1
]}

Yusoff, Siti Fairus M. ^{[1
]}

Yamin, Bohari M. ^{[2
]}

机构：

[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia

[2] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Low Carbon Res Grp, Bangi 43600, Selangor, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2014年 / 70卷

关键词：

data-to-parameter ratio = 19.6; mean σ(C-C) = 0.003 A°; R factor = 0.036; single-crystal X-ray study; T = 296 K; wR factor = 0.086;

D O I：

10.1107/S1600536814008174

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C12H15FN2O2S, the molecule adopts a cis configuration of the fluorobenzoyl group with respect to the thiono group about their C-N bond. The dihedral angle between the fluorobenzoyl group and the thiourea N2CS fragment is 69.60 (11)degrees. An intramolecular N-H center dot center dot center dot O hydrogen bond occurs. In the crystal, molecules form chains along the b-axis direction via O-H center dot center dot center dot S and C-H center dot center dot center dot O hydrogen bonds.

引用

页码：O570 / +

页数：7

共 50 条

[31] Synthesis of N-(2-hydroxyethyl)-substituted piperidines and perhydroquinolines
Golikov, AG
Reshetov, PV
Krivenko, AP
KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1997, (06): : 851 - 852
[32] 2-[Carbamothioyl(2-hydroxyethyl)amino]ethyl benzoate: crystal structure, Hirshfeld surface analysis and computational study
Tan, Sang Loon
Tiekink, Edward R. T.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2020, 76 : 933 - +
[33] Physical and chemical properties of N-(2-hydroxyethyl)alkylamines
A. V. Radushev
D. V. Koltashev
T. Yu. Nasrtdinova
M. G. Shcherban’
L. G. Chekanova
M. D. Plotnikova
Russian Journal of Applied Chemistry, 2010, 83 : 1475 - 1479
[34] Bis[N-(2-hydroxyethyl)-β-alaninato]copper(II)
Pestov, AV
Peresypkina, EV
Virovets, AV
Podberezskaya, NV
Yatluk, YG
Skorik, YA
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2005, 61 : M510 - M512
[35] Physical and Chemical Properties of N-(2-Hydroxyethyl)alkylamines
Radushev, A. V.
Koltashev, D. V.
Nasrtdinova, T. Yu.
Shcherban, M. G.
Chekanova, L. G.
Plotnikova, M. D.
RUSSIAN JOURNAL OF APPLIED CHEMISTRY, 2010, 83 (08) : 1475 - 1479
[36] REACTION OF N-(2-HYDROXYETHYL) AMIDO COMPOUNDS.
Wicks Jr., Zeno W.
Appelt, Marian R.
Soleim, James C.
1600, (57):
[37] CRYSTAL-STRUCTURE OF N-(2-HYDROXYETHYL)-OCTADECANAMIDE
DAHLEN, B
PASCHER, I
SUNDELL, S
ACTA CHEMICA SCANDINAVICA SERIES A-PHYSICAL AND INORGANIC CHEMISTRY, 1977, 31 (04): : 313 - 320
[38] Copolymerization of N-phenylmaleimide with 2-hydroxyethyl and ethyl methacrylates
Senel, S
Rzaev, ZMO
Piskin, E
POLYMER INTERNATIONAL, 2003, 52 (05) : 713 - 721
[39] SYNTHESIS OF N-(2-HYDROXYETHYL)IMINOGLUTARIMIDES FROM N-(2-BROMOETHYL)GLUTARIMIDES
PODONA, T
LAZAR, S
COUDERT, G
GUILLAUMET, G
TETRAHEDRON, 1993, 49 (21) : 4619 - 4626
[40] Spontaneous copolymerization of 3-nitrophthalic anhydride with N-(2-hydroxyethyl)ethyleneimine
Pooley, SA
Canessa, GS
Rivas, BL
Espejo, E
BOLETIN DE LA SOCIEDAD CHILENA DE QUIMICA, 1996, 41 (01): : 71 - 78

← 1 2 3 4 5 →