INVESTIGATION OF PRETREATMENT TECHNIQUES FOR GAS-CHROMATOGRAPHIC DETERMINATION OF TRIBUTYLTIN AND TRIPHENYLTIN COMPOUNDS IN FISH TISSUE

被引：0
|
作者：
KUROSAKI, H
YOKOYAMA, H
OZAKI, K
机构：
来源：
BUNSEKI KAGAKU | 1991年 / 40卷 / 03期
关键词：
DETERMINATION OF TRIBUTYLTIN AND TRIPHENYLTIN COMPOUNDS IN FISH TISSUE; COMPARISON OF EXTRACTION METHOD FROM FISH TISSUE; ANALYSIS BY CAPILLARY COLUMN GC-FLAME PHOTOMETRIC DETECTION; ALKALINE HYDROLYSIS OF FISH TISSUE;
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Five different extraction methods for gas chromatographic determination of tributyltin (TBT) and triphenyltin (TPT) compounds in fish tissue were compared. Analytical results of TBT in the sea bass tissue by 5 different methods varied from 0.013 to 0.098-mu-g g-1 and that of TPT varied from 0.18 to 0.78-mu-g g-1. No interfering peaks were found in the gas chromatograms. The method in which alkaline hydrolysis and extraction with hexane/ethyl acetate/ (1:1, v/v) mixture was used, gave the best analytical results.
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页码：T65 / T69
页数：5
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