Synthesis and Reactions of 2-(N-tetrabromophthalimido) Ethyl Acrylate Polymer with Hydroxy and Amino Compounds

被引：0
|
作者：
Khalil, A. A. [1 ]
机构：
[1] Benha Univ, Fac Sci, Chem Dept, Banha, Egypt
来源：
EGYPTIAN JOURNAL OF CHEMISTRY | 2011年 / 54卷 / 02期
关键词：
N-(2-Hydroxyethyl) tetrabromophthalimide; 2-(N-tetrabromophthalimido) ethyl acrylate; Acryloyl chloride; Exchange reactions and Copolymers;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
N-(2-HYDROXYETHYL) tetrabromophthalimide (HETP) was.. prepared by heating tetrabromophthalic anhydride dissolved in dimethyl formamide (DMF) with ethanol amine. 2-(N-tetrabromophthalimido) ethyl acrylate (TPEA) was prepared by the reaction of acryloyl chloride (AC) with N-(2- hydroxyethyl) tetrabromophthalimide (HETP) in presence of triethyl amine(TEA). The resulting monomer was polymerized. The exchange reactions were carried out in solution at 60 degrees C The structure of prepared polymers and copolymers was investigated by bromine analysis, IR and (HNMR)-H-1 spectroscopy.
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页码：271 / 279
页数：9
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