COMPLETE H-1 AND C-13 NMR SPECTRAL ASSIGNMENT OF PENTACYCLO [6.4.0.0(2,6).0(5,9).0(4,12)]DODECANE DERIVATIVES AND STRUCTURE ELUCIDATION OF PENTACYCLO [6.4.0.0(2,6).0(3,11).0(5,9)]DODECANE

被引：18
|
作者：
MARTINS, FJC
COETZEE, GH
FOURIE, L
VENTER, HJ
VILJOEN, AM
WESSELS, PL
机构：
[1] Department of Chemistry, Potchefstroom University for C.H.E, Potchefstroom
[2] Department of Chemistry, University of Pretoria, Pretoria
来源：
MAGNETIC RESONANCE IN CHEMISTRY | 1993年 / 31卷 / 06期
关键词：
PENTACYCLODODECANE MOLECULES; H-1; NMR; C-13; HOMO NUCLEAR AND HETERONUCLEAR SPI EXPERIMENTS; NOE DIFFERENCE SPECTRA;
D O I：
10.1002/mrc.1260310611
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Treatment of pentacyclo[6,4.0.0(2.6).0(5.9).0(4,12)]dodecan-2-ol with concentrated sulphuric acid produced the rearranged hydrocarbon pentacyclo[6.4.0.0(2,6).0(3,11).0(5,9)]dodecane as the main product. High-field H-1 and C-13 NMR techniques were used in the structure elucidation and assignment of the different NMR resonances of these two and related compounds.
引用
收藏
页码：578 / 584
页数：7
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