Combustion Synthesis of Mo5Si3 in Chemical Furnace

被引:0
|
作者
Gao, J. -Y. [1 ]
Jiang, W. [1 ]
机构
[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, 1295 Dingxi Rd, Shanghai 200050, Peoples R China
关键词
intermetallics; chemical synthesis; crystal structure and symmetry; electron microscopy; x-ray scattering;
D O I
10.3103/S1061386208010056
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The combustion synthesis of Mo5Si3 was carried out in a chemical furnace using 5Ti + 3Si mixtures as a chemical fuel. The synthesized single phase Mo5Si3 exhibited a spatial network microstructure and angular texture of crystals. The chemical composition and crystal morphology of intermediate phases suggest that the formation of Mo5Si3 occurs via dissolution of Mo in the Si melt followed by reactive diffusion in the supersaturated "liquid Si-Mo melt-solid Mo" system.
引用
收藏
页码:49 / 53
页数:5
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