Validation of Bulk Analysis with Simulated Swipe Samples Containing Ultra-Trace Amounts of Uranium and Plutonium Using MC-ICP-MS

被引：5

作者：

Lim, Sang Ho ^{[1
,2
]}

Han, Sun-Ho ^{[1
]}

Park, Jong-Ho ^{[1
,2
]}

Park, Ranhee ^{[1
]}

Lee, Min Young ^{[1
]}

Park, Jinkyu ^{[1
]}

Lee, Chi-Gyu ^{[1
]}

Song, Kyuseok ^{[1
]}

机构：

[1] Korea Atom Energy Res Inst, Nucl Chem Res Div, Daedeok Daero 989-111, Daejeon 34057, South Korea

[2] Univ Sci & Technol, Dept Radiochem & Nucl Nonproliferat, 217 Gajeong-ro, Daejeon 34113, South Korea

来源：

MASS SPECTROMETRY LETTERS | 2015年 / 6卷 / 03期

关键词：

Bulk analysis; Environmental samples; Chemical separation; IDMS; MC-ICP-MS;

D O I：

10.5478/MSL.2015.6.3.75

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC-ICP-MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA)

引用

页码：75 / 79

页数：5