Facile One-Pot Synthesis of Oxo-Xanthenes under Microwave Irradiation

被引：10
|
作者：
Preetam, Amreeta [1 ]
Prasad, Davinder [1 ]
Sharma, Jatin K. [1 ]
Nath, Mahendra [1 ]
机构：
[1] Univ Delhi, Dept Chem, Delhi 110007, India
来源：
CURRENT MICROWAVE CHEMISTRY | 2015年 / 2卷 / 01期
关键词：
9-Aryl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-diones; 9-substituted-2,3,4,9-tetrahydro-1H-xanthen-1-ones; 12-aryl-8,9,10,12-tetrahydrobenzo[a]-xanthene-11-ones; Bronsted acid surfactant combined catalyst; eco-friendly protocol; microwave-assisted synthesis; mild process; multi-component reactions; one-pot methodology; oxo-xanthenes; p-dodecylbenzenesulfonic acid; single crystal XRD data; solvent-free conditions;
D O I：
10.2174/221333560201150212102647
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A convenient diversity oriented synthetic procedure for the construction of various oxo-xanthenes such as 12aryl-8,9,10,12-tetrahydrobenzo[a]- xanthene-11-ones, 9-aryl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-diones and 9substituted- 2,3,4,9-tetrahydro-1H-xanthen-1-ones has been developed by using p-dodecylbenzenesulfonic acid as an efficient Bronsted acid catalyst under solvent-free microwave conditions. The present methodology is found to be operationally simple and demonstrates many advantages including shorter reaction times, easy purification steps and good to excellent yields of the target products.
引用
收藏
页码：15 / 23
页数：9
相关论文
共 50 条
  • [31] One-pot four-component synthesis of pyranopyrazoles under microwave irradiation: A green procedure
    Bandyopadhyay, Debasish
    Pena-Agudelo, Mark
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2015, 249
  • [32] One-pot synthesis of a novel compound N-hydroxydeca-hydroacridine under microwave irradiation
    Tu, SJ
    Fang, F
    Zhu, SL
    Li, TJ
    Zhang, XJ
    Zhuang, QY
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2004, 41 (05) : 767 - 770
  • [33] Efficient One-Pot Synthesis of 3-Amino-7-azaindoles Under Microwave Irradiation
    Yang, Hai-Kui
    You, Wen-Wei
    Yan, Guang-Hua
    Jiang, Zhi-Hong
    Zhao, Pei-Liang
    Zhou, Zhong-Zhen
    [J]. SYNTHETIC COMMUNICATIONS, 2014, 44 (08) : 1165 - 1171
  • [34] A New, One-Pot, Multicomponent Synthesis of Bioactive N-Pyrazolylformamidines under Microwave Irradiation
    Lim, Felicia Phei Lin
    Luna, Giuseppe
    Dolzhenko, Anton V.
    [J]. SYNTHESIS-STUTTGART, 2016, 48 (15): : 2423 - 2428
  • [35] ONE-POT GRAEBE-ULLMANN SYNTHESIS OF GAMMA-CARBOLINES UNDER MICROWAVE IRRADIATION
    MOLINA, A
    VAQUERO, JJ
    GARCIANAVIO, JL
    ALVAREZBUILLA, J
    [J]. TETRAHEDRON LETTERS, 1993, 34 (16) : 2673 - 2676
  • [36] An Effective, One-Pot Synthesis of Fully Substituted Pyridines under Microwave Irradiation in the Absence of Solvent
    Yang, Xiao-Hui
    Zhou, Yong-Hong
    Zhang, Ping-Hu
    Zhang, Li-Yun
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2013, 50 (06) : 1346 - 1350
  • [37] One-pot synthesis of 2-aryl- and 2-alkylbenzothiazoles under microwave irradiation
    Kamila, S
    Zhang, HM
    Biehl, ER
    [J]. HETEROCYCLES, 2005, 65 (09) : 2119 - 2126
  • [38] Zeolite-Supported One-Pot Synthesis of Bis-azetidinones under Microwave Irradiation
    Jetti, Venkateshwarlu
    Pagadala, Ramakanth
    Meshram, Jyotsna S.
    Chopde, Himani N.
    Malladi, Latha
    [J]. JOURNAL OF HETEROCYCLIC CHEMISTRY, 2013, 50 : E160 - E165
  • [39] 'One-pot' synthesis of some pyrazolines and pyrazoles in 'dry media' under microwave irradiation.
    Syassi, B
    Bougrin, K
    Lamiri, M
    Soufiaoui, M
    [J]. NEW JOURNAL OF CHEMISTRY, 1998, 22 (12) : 1545 - 1548
  • [40] One-pot synthesis of nitriles from aldehydes under microwave irradiation: Influence of the medium and mode of microwave irradiation on product formation
    Chakraborti, AK
    Kaur, G
    [J]. TETRAHEDRON, 1999, 55 (46) : 13265 - 13268
12345