PB3U11O36, A RIETVELD REFINEMENT OF NEUTRON POWDER DIFFRACTION DATA

被引:12
|
作者
IJDO, DJW
机构
关键词
D O I
10.1107/S0108270192010874
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Trilead undecauranate, Pb3U11O36, M(r) = 3815.88, orthorhombic, Pmmn. At T = 295 K, a = 28.459 (1), b = 8.3790 (3), c = 6.7650 (3) angstrom, V = 1613.2 (1) angstrom3, Z = 2, D(x) = 7.854 Mg m-3, muR = 0.11, lambda = 2.5700 (1) angstrom, R(p) = 2.94, R(wp) = 3.99%. The structure has been refined by Rietveld analysis of neutron powder diffraction data for 427 reflections. The structure is closely related to alpha-U3O8.
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页码:654 / 656
页数:3
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