DETECTING C-13 IN SOLID PITCHES BY CP/MAS SOLID-STATE NMR

被引：17

作者：

OLLIVIER, P ^{[1
]}

GERSTEIN, BC ^{[1
]}

机构：

[1] IOWA STATE UNIV SCI & TECHNOL,DEPT CHEM,AMES,IA 50011

来源：

CARBON | 1984年 / 22卷 / 4-5期

关键词：

MAGNETIC RESONANCE;

D O I：

10.1016/0008-6223(84)90013-7

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Comparison of **1**3CNMR spectra taken under conditions cross polarization with strong proton decoupling but no sample rotation (CP) and cross polarization with strong proton decoupling and magic angle sample spinning (CP/MAS) indicate that there is a loss of intensity in the aliphatic region and indications of a loss in the aromatic region under MAS. This effect is discussed.

引用

页码：409 / 412

页数：4

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