DETECTING C-13 IN SOLID PITCHES BY CP/MAS SOLID-STATE NMR

被引：17
|
作者：
OLLIVIER, P [1 ]
GERSTEIN, BC [1 ]
机构：
[1] IOWA STATE UNIV SCI & TECHNOL,DEPT CHEM,AMES,IA 50011
来源：
CARBON | 1984年 / 22卷 / 4-5期
关键词：
MAGNETIC RESONANCE;
D O I：
10.1016/0008-6223(84)90013-7
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Comparison of **1**3CNMR spectra taken under conditions cross polarization with strong proton decoupling but no sample rotation (CP) and cross polarization with strong proton decoupling and magic angle sample spinning (CP/MAS) indicate that there is a loss of intensity in the aliphatic region and indications of a loss in the aromatic region under MAS. This effect is discussed.
引用
收藏
页码：409 / 412
页数：4
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