Luminol-K3Fe(CN)(6) chemiluminescence system for the determination of glipizide

被引：6
|
作者：
Chen, Xin [1 ]
Xing, Li-Li [2 ]
Tang, Yu-Hai [2 ]
Zhang, Guang-Bin [2 ]
机构：
[1] 405 Hosp Hanzhong City, Hanzhong 723312, Shaanxi, Peoples R China
[2] Xi An Jiao Tong Univ, Inst Analyt Sci, Xian 710061, Shaanxi, Peoples R China
来源：
JOURNAL OF PHARMACEUTICAL ANALYSIS | 2013年 / 3卷 / 02期
关键词：
Luminol-K3Fe(CN)(6); Glipizide; Flow injection; Chemiluminescence;
D O I：
10.1016/j.jpha.2012.07.002
中图分类号：
R9 [药学];
学科分类号：
1007 ;
摘要：
A rapid and sensitive flow-injection chemiluminescence (CL) method for the determination of glipizide was developed on the basis of finding that glipizide can enhance the CL intensity of the luminol-K3Fe(CN)(6) system. In optimum condition, the increased CL intensity was directly proportional to the concentration of glipizide in the range from 4.0 x 10 (8) g/mL to 1.0 x 10 (6) g/ mL and the detection limit was 1.0 x 10 (-8) g/mL glipizide. The relative standard deviation (RSD) of the developed method was 2.1% with 11 repeated measurements of 1.0 x 10(-7) g/mL glipizide. The developed method has been successfully applied to the analysis of glipizide in its pharmaceutical preparations. (C) 2013 Xi'an Jiaotong University. Production and hosting by Elsevier B.V. All rights reserved.
引用
收藏
页码：127 / 131
页数：5
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