LOW-TEMPERATURE MICRO-CALORIMETRY BY DIFFERENTIAL SCANNING

被引：6
|
作者：
RAHM, U [1 ]
GMELIN, E [1 ]
机构：
[1] MAX PLANCK INST FESTKORPERFORSCH,W-7000 STUTTGART 80,GERMANY
来源：
JOURNAL OF THERMAL ANALYSIS | 1992年 / 38卷 / 03期
关键词：
DIFFERENTIAL MICROCALORIMETER; HEAT CAPACITY;
D O I：
10.1007/BF01915498
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
We describe the construction, operation and performance of a fully automated low temperature differential micro-calorimeter for heat capacity measurements on small samples (m < 100 mg) in the temperature range from 15 K to 300 K. The instrument is operated using different calorimetric methods, in particular adiabatic differential scanning. Its reliability is demonstrated by measuring the heat capacity of 23 mg of copper and 37 mg of cyclopentane with an error of less than 2%.
引用
收藏
页码：335 / 344
页数：10
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