Synthesis and Characterization of Green Porous Carbons with Large Surface Area by Two Step Chemical Activation with KOH

被引:0
|
作者
Nasri, Noor Shawal [1 ]
Jibril, Mohammed [1 ,2 ,3 ]
Zaini, Muhammad Abbas Ahmad [2 ]
Mohsin, Rahmat [1 ]
Dadum, Hamza Usman [1 ,2 ,3 ]
Musa, Ahmed Murtala [1 ]
机构
[1] Univ Teknol Malaysia, UTM MPRC Inst Oil & Gas Energy Res Alliance, Sustainable Waste To Wealth Unit, Utm Johor Bahru 81310, Johor, Malaysia
[2] Univ Teknol Malaysia, Fac Chem Engn, Johor Baharu 81310, Johor, Malaysia
[3] Abubakar Tafawa Balewa Univ, Chem Engn Programme, Bauchi 0248, Nigeria
来源
JURNAL TEKNOLOGI | 2014年 / 67卷 / 04期
关键词
Adsorbent; coconut shell; micropores; synthesis; chemical activation; potassium hydroxide;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Porous carbons were synthesized from coconut shell using chemical activation by potassium hydroxide (KOH). N-2 adsorption isotherm analysis for BET surface area and pore volume of the synthesized porous carbon were carried out. The Langmuir surface area, BET surface area and pore volume are 1646 m(2)/g, 1353 m(2)/g and 0.6 cm(3)/g, respectively. From the FTIR analysis, hydroxyls, alkenes, carbonyls and aromatics functional groups were identified. The proximate and ultimate analysis shows high percentage of carbon and less ash content which indicates a good precursor material for porous carbon. The carbonization temperature and time were also varied to observe their effect on the yield of char, with carbonization at 7000C for 2 h having highest yield of 32%.
引用
收藏
页数:4
相关论文
共 50 条
  • [21] Benzene and Methane Adsorption on Ultrahigh Surface Area Carbons Prepared from Sulphonated Styrene Divinylbenzene Resin by KOH Activation
    Choma, Jerzy
    Osuchowski, Lukasz
    Dziura, Aleksandra
    Marszewski, Michal
    Jaroniec, Mietek
    ADSORPTION SCIENCE & TECHNOLOGY, 2015, 33 (6-8) : 587 - 594
  • [22] Co-gelation synthesis of porous graphitic carbons with high surface area and their applications
    Wang, Zhongli
    Zhang, Xinbo
    Liu, Xiaojuan
    Lv, Minfeng
    Yang, Kuiyue
    Meng, Jian
    CARBON, 2011, 49 (01) : 161 - 169
  • [23] Synthesis of magnetic biochar with high iron content and large specific surface area: Synergistic effect of Fe doping and KOH activation
    Sun, Mengchao
    Wang, Chu
    Luo, Zejun
    Zhu, Xifeng
    JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS, 2023, 173
  • [24] Novel silica-sol mediated synthesis of high surface area porous carbons
    Han, SJ
    Hyeon, T
    CARBON, 1999, 37 (10) : 1645 - 1647
  • [25] Synthesis of a porous chromium fluoride catalyst with a large surface area
    Quan, HD
    Yang, HE
    Tamura, M
    Sekiya, A
    JOURNAL OF CATALYSIS, 2005, 231 (01) : 254 - 257
  • [26] Synthesis of mesopore-dominated porous carbon with ultra-high surface area via urea-assisted KOH activation
    Zheng, Liang
    Wang, Huimei
    Wang, Xiaohui
    Liu, Yu
    Liu, Zhong
    Wang, Shoujuan
    Lin, Yaofeng
    JOURNAL OF WOOD CHEMISTRY AND TECHNOLOGY, 2023, 43 (02) : 78 - 91
  • [27] Porous carbon with a large surface area and an ultrahigh carbon purity via templating carbonization coupling with KOH activation as excellent supercapacitor electrode materials
    Sun, Fei
    Gao, Jihui
    Liu, Xin
    Pi, Xinxin
    Yang, Yuqi
    Wu, Shaohua
    APPLIED SURFACE SCIENCE, 2016, 387 : 857 - 863
  • [28] Formation of High Surface Area Hierarchical Porous Carbon Via a Novel Two Step Activation Process for Fast Supercapacitors
    Li, Guangli
    Wei, Xing
    Li, Yingying
    Mao, Wenfeng
    Du, Guixiang
    Zhang, Jingbo
    CHEMISTRYSELECT, 2020, 5 (06): : 2008 - 2014
  • [29] Study on synthesis of low surface area activated carbons using multi-step activation for use in electric double layer capacitor
    Roh, Kwang Chul
    Park, Jin Bae
    Lee, Chul-Tae
    Park, Chul Wan
    JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2008, 14 (02) : 247 - 251
  • [30] Adsorption Properties of Micro-/Meso-porous Carbons Obtained by Colloidal Templating and Post-synthesis KOH Activation
    Choma, Jerzy
    Dziura, Aleksandra
    Gorka, Joanna
    Jaroniec, Mietek
    ADSORPTION SCIENCE & TECHNOLOGY, 2011, 29 (05) : 457 - 465