Synthesis and Characterization of Green Porous Carbons with Large Surface Area by Two Step Chemical Activation with KOH

被引:0
|
作者
Nasri, Noor Shawal [1 ]
Jibril, Mohammed [1 ,2 ,3 ]
Zaini, Muhammad Abbas Ahmad [2 ]
Mohsin, Rahmat [1 ]
Dadum, Hamza Usman [1 ,2 ,3 ]
Musa, Ahmed Murtala [1 ]
机构
[1] Univ Teknol Malaysia, UTM MPRC Inst Oil & Gas Energy Res Alliance, Sustainable Waste To Wealth Unit, Utm Johor Bahru 81310, Johor, Malaysia
[2] Univ Teknol Malaysia, Fac Chem Engn, Johor Baharu 81310, Johor, Malaysia
[3] Abubakar Tafawa Balewa Univ, Chem Engn Programme, Bauchi 0248, Nigeria
来源
JURNAL TEKNOLOGI | 2014年 / 67卷 / 04期
关键词
Adsorbent; coconut shell; micropores; synthesis; chemical activation; potassium hydroxide;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Porous carbons were synthesized from coconut shell using chemical activation by potassium hydroxide (KOH). N-2 adsorption isotherm analysis for BET surface area and pore volume of the synthesized porous carbon were carried out. The Langmuir surface area, BET surface area and pore volume are 1646 m(2)/g, 1353 m(2)/g and 0.6 cm(3)/g, respectively. From the FTIR analysis, hydroxyls, alkenes, carbonyls and aromatics functional groups were identified. The proximate and ultimate analysis shows high percentage of carbon and less ash content which indicates a good precursor material for porous carbon. The carbonization temperature and time were also varied to observe their effect on the yield of char, with carbonization at 7000C for 2 h having highest yield of 32%.
引用
收藏
页数:4
相关论文
共 50 条
  • [1] Synthesis and Characterization of Bio-Based Porous Carbons by Two Step Physical Activation with CO2
    Nasri, Noor Shawal
    Jibril, Mohammed
    Zaini, Muhammad Abbas Ahmad
    Mohsin, Rahmat
    Dadum, Hamza Usman
    Musa, Ahmed Murtala
    JURNAL TEKNOLOGI, 2014, 68 (05):
  • [2] High-surface-area porous carbons produced by the mild KOH activation of a chitosan hydrochar and their CO2 capture
    Wang, Jing
    Chen, Shuang
    Xu, Jia-Yu
    Liu, Li-Cheng
    Zhou, Ji-Cheng
    Cai, Jin-Jun
    Xinxing Tan Cailiao/New Carbon Materials, 2021, 36 (06): : 1081 - 1093
  • [3] High-surface-area porous carbons produced by the mild KOH activation of a chitosan hydrochar and their CO2 capture
    Wang, Jing
    Chen, Shuang
    Xu, Jia-yu
    Liu, Li-cheng
    Zhou, Ji-cheng
    Cai, Jin-jun
    NEW CARBON MATERIALS, 2021, 36 (06) : 1081 - 1093
  • [4] A microscopic view of physical and chemical activation in the synthesis of porous carbons
    Paredes, J. I.
    Suarez-Garcia, F.
    Martinez-Alonso, A.
    Tascon, J. M. D.
    LANGMUIR, 2006, 22 (23) : 9730 - 9739
  • [5] Preparation and characterization of porous carbons from PAN-based preoxidized cloth by KOH activation
    Wu, MB
    Zha, QF
    Qiu, JS
    Guo, YS
    Shang, HY
    Yuan, AJ
    CARBON, 2004, 42 (01) : 205 - 210
  • [6] Role of KCl in activation mechanisms of KOH-chemically activated high surface area carbons
    Campello Gomez, Ignacio
    Cruz Jr, Orlando F.
    Silvestre-Albero, Joaquin
    Rambo, Carlos R.
    Escandell, Manuel Martinez
    JOURNAL OF CO2 UTILIZATION, 2022, 66
  • [7] Preparation of high surface area activated carbons by KOH activation promoted by alkali metal halides
    Liu Xin-mei
    Dai Xiao-dong
    Zhang Jian
    Song hui
    Yan Zi-feng
    NEW CARBON MATERIALS, 2008, 23 (02) : 133 - 138
  • [8] Preparation of high surface area activated carbons by KOH activation promoted by alkali metal halides
    Liu, Xin-Mei
    Dai, Xiao-Dong
    Zhang, Jian
    Song, Hui
    Yan, Zi-Feng
    Xinxing Tan Cailiao/ New Carbon Materials, 2008, 23 (02): : 133 - 138
  • [9] Synthesis and electrochemical characterization of mesoporous carbons prepared by chemical activation
    Zhao, Jiachang
    Dai, Yang
    Xu, Jingli
    Chen, Sihao
    Xie, Jingying
    JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2008, 155 (07) : A475 - A480
  • [10] High surface area porous carbons produced by steam activation of graphene aerogels
    Sui, Zhu-Yin
    Meng, Qing-Han
    Li, Ji-Tao
    Zhu, Jian-Hua
    Cui, Yi
    Han, Bao-Hang
    JOURNAL OF MATERIALS CHEMISTRY A, 2014, 2 (25) : 9891 - 9898