The study of thermal decomposition of RDX by corona discharge-ion mobility spectrometry-mass spectrometry

被引：3

作者：

Lichvanova, Zuzana ^{[1
]}

Sabo, Martin ^{[1
]}

Matejcik, Stefan ^{[1
]}

机构：

[1] Comenius Univ, Fac Math Phys & Informat, Dept Expt Phys, Mlynska Dolina F2, Bratislava 84248, Slovakia

来源：

INTERNATIONAL JOURNAL FOR ION MOBILITY SPECTROMETRY | 2015年 / 18卷 / 1-2期

关键词：

Corona discharge; Negative ions; Ion mobility spectrometry; Mass spectrometry; Thermal decomposition; RDX;

D O I：

10.1007/s12127-015-0169-9

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

In this study we have examined the formation of ions from hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) sample evaporated at 473 K in reactions with reactant ions (RI) produced in negative corona discharge (CD). The ions have been analysed and detected by ion mobility spectrometry coupled to orthogonal acceleration time of flight spectrometer (IMS-oaTOF). The chemical ionisation was carried out by O-2(-), O-2(-) (H2O), N2O2-, N2O3- and N2O3- (H2O) RI formed in CD operated in zero air in the reverse gas flow mode at elevated temperatures 438 K and by Cl-(H2O) n (n= 0,1,2) at 332K. In case of 332K, theRIwere prepared by admixture of carbon tetrachloride (CCl4 - dopant gas) in order to enhance sensitivity of RDX.

引用

页码：59 / 66

页数：8

共 50 条

[21] Limitations of ion mobility spectrometry-mass spectrometry for the relative quantification of architectural isomeric polymers: A case study
Lienard, Romain
Duez, Quentin
Grayson, Scott M.
Gerbaux, Pascal
Coulembier, Olivier
De Winter, Julien
RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2020, 34
[22] Letter: A simple ion source set-up for desorption/ionization on silicon with ion mobility spectrometry and ion mobility spectrometry-mass spectrometry
Adamov, Alexey
Sysoev, Alexey A.
Grigoras, Kestutis
Laakia, Jaakko
Kotiaho, Tapio
EUROPEAN JOURNAL OF MASS SPECTROMETRY, 2011, 17 (06) : 593 - 597
[23] Improving the Speed and Selectivity of Newborn Screening Using Ion Mobility Spectrometry-Mass Spectrometry
Dodds, James N.
Baker, Erin S.
ANALYTICAL CHEMISTRY, 2021, 93 (51) : 17094 - 17102
[24] Advances in ion mobility spectrometry-mass spectrometry reveal key insights into amyloid assembly
Woods, L. A.
Radford, S. E.
Ashcroft, A. E.
BIOCHIMICA ET BIOPHYSICA ACTA-PROTEINS AND PROTEOMICS, 2013, 1834 (06): : 1257 - 1268
[25] Architectural Differentiation of Linear and Cyclic Polymeric Isomers by Ion Mobility Spectrometry-Mass Spectrometry
Hoskins, Jessica N.
Trimpin, Sarah
Grayson, Scott M.
MACROMOLECULES, 2011, 44 (17) : 6915 - 6918
[26] Determining the topology of virus assembly intermediates using ion mobility spectrometry-mass spectrometry
Knapman, Tom W.
Morton, Victoria L.
Stonehouse, Nicola J.
Stockley, Peter G.
Ashcroft, Alison E.
RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2010, 24 (20) : 3033 - 3042
[27] Structures of Metallosupramolecular Coordination Assemblies Can Be Obtained by Ion Mobility Spectrometry-Mass Spectrometry
Brocker, Erin R.
Anderson, Stanley E.
Northrop, Brian H.
Stang, Peter J.
Bowers, Michael T.
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2010, 132 (38) : 13486 - 13494
[28] High-Resolution Ion Mobility Spectrometry-Mass Spectrometry on Poly(methyl methacrylate)
Song, Junkan
Grun, Christian H.
Heeren, Ron M. A.
Janssen, Hans-Gerd
van den Brink, Oscar F.
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2010, 49 (52) : 10168 - 10171
[29] Distinguishing Protein Chemical Topologies Using Supercharging Ion Mobility Spectrometry-Mass Spectrometry
Lee, Jiyeon
Im, Dahye
Liu, Yajie
Fang, Jing
Tian, Xibao
Kim, Minsu
Zhang, Wen-Bin
Seo, Jongcheol
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2023, 62 (51)
[30] Experimental simulation of negative ion chemistry in Martian atmosphere using ion mobility spectrometry-mass spectrometry
Martin Sabo
Zuzana Lichvanová
Juraj Orszagh
Nigel Mason
Štefan Matejčík
The European Physical Journal D, 2014, 68

← 1 2 3 4 5 →