CHIRAL NUCLEAR MAGNETIC-RESONANCE SOLVATING AGENTS - RESOLUTION, DETERMINATION OF ENANTIOMERIC PURITY, AND ASSIGNMENT OF ABSOLUTE-CONFIGURATION OF CYCLIC AND ACYCLIC SULFINATE ESTERS

被引：111

作者：

PIRKLE, WH ^{[1
]}

HOEKSTRA, MS ^{[1
]}

机构：

[1] UNIV ILLINOIS,SCH CHEM SCI,URBANA,IL 61801

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1976年 / 98卷 / 07期

关键词：

D O I：

10.1021/ja00423a031

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

引用

页码：1832 / 1839

页数：8

共 48 条

[41] USE OF SHIFT-REAGENT WITH MTPA DERIVATIVES IN H NMR-SPECTROSCOPY .6. DETERMINATION OF ABSOLUTE-CONFIGURATION AND ENANTIOMERIC PURITY OF 2-HYDROXYCARBOXYLIC AND 3-HYDROXYCARBOXYLIC ACID-ESTERS
YASUHARA, F
YAMAGUCHI, S
TETRAHEDRON LETTERS, 1980, 21 (29) : 2827 - 2830
[42] USE OF SHIFT-REAGENT WITH MTPA DERIVATIVES IN H-1 NMR-SPECTROSCOPY .3. DETERMINATION OF ABSOLUTE-CONFIGURATION AND ENANTIOMERIC PURITY OF PRIMARY CARBINOLS WITH CHIRAL CENTER AT C-2 POSITION
YASUHARA, F
YAMAGUCHI, S
TETRAHEDRON LETTERS, 1977, (47) : 4085 - 4088
[43] RESOLUTION AND ABSOLUTE-CONFIGURATION OF 1,2,3,5,6,10B-BETA-HEXAHYDRO-6-ALPHA-PHENYLPYRROLO[2,1-A]ISOQUINOLINE (MCN-4612-Z) - A PROBLEM OF DETERMINATION OF THE ENANTIOMERIC PURITY FOR A TERTIARY AMINE
MARYANOFF, BE
MCCOMSEY, DF
JOURNAL OF HETEROCYCLIC CHEMISTRY, 1985, 22 (03) : 911 - 914
[44] INFLUENCE OF THE CONFIGURATION OF AN ASYMMETRIC CARBON CENTER ON THE PARAMETERS OF THE NUCLEAR MAGNETIC RESONANCE SPECTRA OF INHERENTLY CHIRAL N-(1-PHENYLETHYL)AMIDES OF CALIX[4]ARENE ACETIC ACIDS: DETERMINATION OF THE ABSOLUTE STEREOCHEMICAL CONFIGURATION OF THE MACROCYCLE
Yesypenko, O. A.
Trybrat, O. O.
Vashchenko, O. O.
Suikov, S. Yu
THEORETICAL AND EXPERIMENTAL CHEMISTRY, 2022, 58 (01) : 54 - 60
[45] Influence of the Configuration of an Asymmetric Carbon Center on the Parameters of the Nuclear Magnetic Resonance Spectra of Inherently Chiral N-(1-Phenylethyl)Amides of Calix[4]Arene Acetic Acids: Determination of the Absolute Stereochemical Configuration of the Macrocycle
O. A. Yesypenko
O. O. Trybrat
O. O. Vashchenko
S. Yu. Suikov
Theoretical and Experimental Chemistry, 2022, 58 : 54 - 60
[46] OPTICALLY-ACTIVE 9-MEMBERED RINGS INCORPORATING THE 8-POSITIONS AND 8'-POSITIONS OF 1,1'-BINAPHTHYL .2. OXYGEN, SULFUR, AND SELENIUM HETEROCYCLES - SYNTHESIS, H-1 NUCLEAR MAGNETIC-RESONANCE SPECTRA, AND ABSOLUTE-CONFIGURATION
HARRIS, MM
PATEL, PK
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1978, (04): : 304 - 307
[47] CONFIGURATION OF OPTICALLY-ACTIVE PHOSPHORUS THIO ACIDS .4. H-1, P-31, AND C-13 NUCLEAR MAGNETIC-RESONANCE NONEQUIVALENCE OF DIASTEREOMERIC SALTS OF CHIRAL PHOSPHORUS THIO ACIDS WITH OPTICALLY-ACTIVE AMINES - METHOD FOR DETERMINING OPTICAL PURITY AND CONFIGURATION OF CHIRAL PHOSPHORUS THIO ACIDSD
MIKOLAJCZYK, M
OMELANCZUK, J
LEITLOFF, M
DRABOWICZ, J
EJCHART, A
JURCZAK, J
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1978, 100 (22) : 7003 - 7008
[48] STRUCTURAL REQUIREMENTS IN CHIRAL DIPHOSPHINERHODIUM COMPLEXES .9. H-1 NUCLEAR MAGNETIC-RESONANCE DETERMINATION OF E,Z-CONFIGURATION AND CIS,TRANS-AMIDE CONFORMATIONS IN PROCHIRAL SUBSTRATES USED IN ASYMMETRIC HYDROGENATION REACTIONS - METHYL AND ETHYL ALPHA-FORMAMIDO-BETA-SUBSTITUTED ACRYLATES
GLASER, R
GERESH, S
SCHOLLKOPF, U
MEYER, R
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1979, (07): : 1746 - 1750

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