4-Phenyl-1,2,4-triazaspiro[4.5] dec-1-ene-3-thione

被引：2
|
作者：
Akkurt, Mehmet [1 ]
Mague, Joel T. [2 ]
Mohamed, Shaaban K. [3 ]
Hassan, Alaa A. [3 ]
Albayati, Mustafa R. [4 ]
机构：
[1] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey
[2] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[3] Mini Univ, Fac Sci, Chem Dept, El Minia 61519, Egypt
[4] Kirkuk Univ, Coll Sci, Dept Chem, Kirkuk, Iraq
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词：
data-to-parameter ratio = 20.6; meanω(C - C) = 0.002 A °; Rfactor = 0.042; single-crystal X-ray study; T = 150 K; wRfactor = 0.104;
D O I：
10.1107/S1600536813019120
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C13H15N3S, the 4,5-dihydro-3H-1,2,4-triazolering is nearly planar [maximum deviation = 0.020 (1) angstrom], while the cyclohexane ring adopts a chair conformation. The dihedral angle between the 4,5-dihydro3H-1,2,4-triazole ring and the phenyl ring is 74.68 (7)degrees. No specific intermolecular interactions are discerned in the crystal packing.
引用
收藏
页码：O1259 / +
页数：7
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