4-Phenyl-1,2,4-triazaspiro[4.5] dec-1-ene-3-thione

被引：2
|
作者：
Akkurt, Mehmet [1 ]
Mague, Joel T. [2 ]
Mohamed, Shaaban K. [3 ]
Hassan, Alaa A. [3 ]
Albayati, Mustafa R. [4 ]
机构：
[1] Erciyes Univ, Fac Sci, Dept Phys, TR-38039 Kayseri, Turkey
[2] Manchester Metropolitan Univ, Chem & Environm Div, Manchester M1 5GD, Lancs, England
[3] Mini Univ, Fac Sci, Chem Dept, El Minia 61519, Egypt
[4] Kirkuk Univ, Coll Sci, Dept Chem, Kirkuk, Iraq
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2013年 / 69卷
关键词：
data-to-parameter ratio = 20.6; meanω(C - C) = 0.002 A °; Rfactor = 0.042; single-crystal X-ray study; T = 150 K; wRfactor = 0.104;
D O I：
10.1107/S1600536813019120
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C13H15N3S, the 4,5-dihydro-3H-1,2,4-triazolering is nearly planar [maximum deviation = 0.020 (1) angstrom], while the cyclohexane ring adopts a chair conformation. The dihedral angle between the 4,5-dihydro3H-1,2,4-triazole ring and the phenyl ring is 74.68 (7)degrees. No specific intermolecular interactions are discerned in the crystal packing.
引用
收藏
页码：O1259 / +
页数：7
相关论文
共 50 条
  • [1] 4-Phenyl-1,2,4-triazaspiro[4.6]undec-1-ene-3-thione
    Mohamed, Shaaban K.
    Mague, Joel T.
    Akkurt, Mehmet
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O640 - +
  • [2] 4-Phenyl-1,2,4-triazaspiro[4.4] non-1-ene-3-thione
    Mague, Joel T.
    Mohamed, Shaaban K.
    Akkurt, Mehmet
    Hassan, Alaa A.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O433 - +
  • [3] Microwave Facilitated Discovery of Substituted 1,2,4-triazaspiro[4.5] dec-2-en-3-amines: Biological and Computational Investigations
    Patel, Parth P.
    Patel, Navin B.
    Tople, Manesh S.
    Patel, Vatsal M.
    Solanki, Mitesh B.
    CURRENT MICROWAVE CHEMISTRY, 2023, 10 (02) : 208 - 222
  • [4] 3-PIPERIDONE DERIVATIVES .4. 1-OXO-4-PHENYL-7-BENZYL-2,4,7-TRIAZASPIRO[4.5]DEC-2-ENE
    OZDOWSKA, Z
    POLISH JOURNAL OF CHEMISTRY, 1982, 56 (4-6) : 811 - 813
  • [5] 5-(3-Methylphenoxymethyl)-4-phenyl-1,2,4-triazole-3-thione
    Wei, Tai-Bao
    Luo, Rong
    Liu, Hong
    Zhang, You-Ming
    Lu, Tong-Bu
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O5883 - O5884
  • [6] 3-(2-chlorophenyl)-4-phenyl-1,2,4-triazole-5-thione
    Kumaran, D
    Ponnuswamy, MN
    Jayanthi, G
    Ramakrishnan, VT
    Chinnakali, K
    Fun, HK
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 581 - 582
  • [7] Synthesis of 2-(4′-(3"-chlorobenzyloxy)-phenyl)-1,3,4-oxadiazolin-5-thione, 3-{4′-(3"-chlorobenzyloxy)-phenyl}-4-phenyl-1,2,4-triazolin-5-thione and their derivatives as potential antileishmanial agents
    Tiwari, R. K.
    Rastogi, Nisheeth
    Sethi, Ralkesh
    Varma, R. S.
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2007, 17 (02) : 177 - 182
  • [8] N-(3,4-Dimethoxyphenyl)-4-oxo-2,3,7-triazaspiro[4.5] dec-1-ene1-carboxamide Hydrochloride
    Srinivasan, Rajagopalan
    Narayana, Badiadka
    Samshuddin, Seranthimata
    Sarojini, Balladka Kunhanna
    MOLBANK, 2012, (03)
  • [9] tert-Butyl 1-(Furan-2-yl)-4-oxo-2,3,7-triazaspiro[4.5]dec-1-ene-7-carboxylate
    Srinivasan, Rajagopalan
    Narayana, Badiadka
    Samshuddin, Seranthimata
    Sarojini, Balladka Kunhanna
    MOLBANK, 2012, (02)
  • [10] 3-(4-phenyl-1,2,4-triazol-3-yl)chromones
    Shokol, TV
    Turov, VA
    Turov, AV
    Kryvokhyzha, NV
    Semenyuchenko, VV
    Khilya, VP
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2005, (11): : 1676 - 1684
12345