COMPLETE C-13 AND H-1-NMR CHEMICAL-SHIFT ASSIGNMENTS OF 1-NITROPYRENE

被引：3

作者：

CHO, BP

LEVINE, RA

EVANS, FE

机构：

[1] National Center for Toxicological Research, HFT-110 Food and Drug Administration, Jefferson

来源：

SPECTROSCOPY LETTERS | 1991年 / 24卷 / 01期

关键词：

1-NITROPYRENE; 2-DIMENSIONAL NMR; LONG-RANGE HETERONUCLEAR CHEMICAL SHIFT CORRELATION; BILINEAR ROTATIONAL DECOUPLING;

D O I：

10.1080/00387019108018119

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

Ambiguities in the C-13 NMR chemical shift assignments of 1-nitropyrene were resolved using direct and long-range two-dimensional heteronuclear chemical shift correlation experiments. The latter was modified with a bilinear rotational decoupling (BIRD) pulse sequence, which enabled detection of all three-bond long-range correlations.

引用

页码：1 / 7

页数：7

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