Synthesis and structure of aryl(hetaryl)spiropyrrolidones

被引：0
|
作者：
V. M. Berestovitskaya
I. A. Litvinov
O. S. Vasil’eva
A. A. Nikonorov
E. S. Ostroglyadov
D. B. Krivolapov
机构：
[1] A. I. Herzen State Pedagogical University of Russia,A. E. Arbuzov Institute of Organic and Physical Chemistry
[2] Kazan Scientific Center of the Russian Academy of Sciences,undefined
来源：
Russian Chemical Bulletin | 2012年 / 61卷
关键词：
2-pyrrolidones; 3,3′-spiropyrrolidones; diastereomers; catalytic hydrogenation;
D O I：
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中图分类号：
学科分类号：
摘要：
Hydrogenation of the diastereouniform 3-[1-aryl(hetaryl)-2-nitroethyl]-3-methoxycarb-onyl-4-phenyl(3-pyridyl)-2-pyrrolidones is accompanied by intramolecular acylation of the formed amino group to afford the diastereomerically pure 4,4′-aryl(hetaryl)-3,3′-spirobi-[2-pyrrolidones]. The structures of these diastereomers were characterized by IR, 1H and 13C NMR spectroscopy using heteronuclear correlation experiments, and X-ray diffraction study.
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页码：1014 / 1023
页数：9
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