Comprehensive Analytical Method for Semi-volatile Organic Compounds in Water Samples by Combination of Disk-type Solid-phase Extraction and Gas Chromatography-Mass Spectrometry Database System

被引：0
|
作者：
Daisuke Jinya
Tomomi Iwamura
Kiwao Kadokami
机构：
[1] Kitakyushu City Institute of Environmental Sciences,Faculty of Environmental Engineering
[2] The University of Kitakyushu,undefined
来源：
Analytical Sciences | 2013年 / 29卷
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摘要：
A disk-type solid-phase extraction method for simultaneous extraction of a wide range of semi-volatile organic compounds in water samples was developed. The developed method could extract 186 out of 202 model compounds from spiked environmental samples (0.1 μg/L) with 94% average recovery (50 - 111%). Compared with the previous cartridge-type method, the extraction time was reduced to approximately 1/6. Applying the combination of the developed method and the database system to environmental samples for non-target analyses, 39 micro-pollutants with a wide range of physicochemical properties were determined.
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页码：483 / 486
页数：3
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