Crystal structure of N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropane

被引：0
|
作者：
A. D. Khalaji
K. Fejfarova
M. Dusek
机构：
[1] Golestan University,Department of Chemistry, Faculty of Science
[2] Institute of Physics of the ASCR,undefined
来源：
Journal of Structural Chemistry | 2011年 / 52卷
关键词：
X-ray diffraction; orthorhombic symmetry; Schiff base;
D O I：
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学科分类号：
摘要：
The Schiff-base compound N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropan, (2,5-MeO-ba)2pn, is synthesized and characterized by elemental analysis, FT-IR and 1H NMR spectroscopy. The crystal structure of (2,5-MeO-ba)2pn is determined by X-ray single crystal diffraction analysis. The X-ray diffraction analysis at 120 K reveals that (2,5-MeO-ba)2pn crystallizes in the orthorhombic system, Fdd2 space group with a = 29.339(9) Å, b = 29.4073(11) Å, c = 4.4524(2) Å, V = 3840.8(3) Å3, μ = 0.72 mm−1, and Z = 8.
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页码：1131 / 1133
页数：2
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