Analysis of Para Red and Sudan Dyes in Egg Yolk by UPLC–MS–MS

被引:13
|
作者
Xiaolin Hou
Yonggang Li
Shoujun Cao
Zhongwen Zhang
Yongnin Wu
机构
[1] Beijing University of Agriculture,Department of Animal Science
[2] Ministry of Business,Circulation Industry Promotion Center
[3] Beijing Vocational College of Agriculture,Department of Animal Science
[4] Chinese Center for Disease Control and Prevention,Institute of Nutrition and Food Hygiene
来源
Chromatographia | 2010年 / 71卷
关键词
Column liquid chromatography; UPLC–MS–MS; Matrix solid-phase dispersion; Para red; Sudan dyes;
D O I
暂无
中图分类号
学科分类号
摘要
Matrix solid-phase dispersion (MSPD) with alumina N as adsorbent has been used for extraction of para red, Sudan 1, Sudan 2, Sudan 3, and Sudan 4 dyes from egg yolk. The extracts were analyzed by ultra-performance liquid chromatography–tandem mass spectrometry (UPLC–MS–MS). Mean recovery for the five dyes ranged from 63.2 to 98.6%, with CV 0.55–10.00%. One sample was confirmed to contain 0.3 mg kg−1 Sudan 4.
引用
收藏
页码:135 / 138
页数:3
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